Corrosion of carbon steel caustic header in the presence of chloride ions

Caustic soda produced in caustic cells at a petrochemical plant was loaded into a crude tank by means of a caustic header line made of plain carbon steel. After a fraction of expected service life, the header was severely corroded. Scanning electron microscopy (SEM) coupled with energy dispersive X-...

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Main Author: Ul-Hamid, Anwar (author)
Other Authors: unknown (author)
Format: article
Published: 2020
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Online Access:https://eprints.kfupm.edu.sa/id/eprint/136056/1/anwar_Corrosion_carbon_steel_caustic_header_the_presence_of_chloride_ions.pdf
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author Ul-Hamid, Anwar
author2 unknown
author2_role author
author_facet Ul-Hamid, Anwar
unknown
author_role author
dc.creator.none.fl_str_mv Ul-Hamid, Anwar
unknown
dc.date.*.fl_str_mv 2020
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://eprints.kfupm.edu.sa/id/eprint/136056/1/anwar_Corrosion_carbon_steel_caustic_header_the_presence_of_chloride_ions.pdf
Corrosion of carbon steel caustic header in the presence of chloride ions. Engineering Failure Analysis.
dc.language.none.fl_str_mv en
dc.relation.none.fl_str_mv https://eprints.kfupm.edu.sa/id/eprint/136056/
dc.rights.*.fl_str_mv info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Corrosion
dc.title.none.fl_str_mv Corrosion of carbon steel caustic header in the presence of chloride ions
dc.type.none.fl_str_mv Article
PeerReviewed
info:eu-repo/semantics/publishedVersion
info:eu-repo/semantics/article
description Caustic soda produced in caustic cells at a petrochemical plant was loaded into a crude tank by means of a caustic header line made of plain carbon steel. After a fraction of expected service life, the header was severely corroded. Scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDS) and X-ray diffraction (XRD) was used to identify the material and the corrosion product. Metallurgical evaluation suggested that the mode of failure was localized attack by chlorine and/or hydrochloric acid at pipe connections (flanges) where concentrated solutions could accumulate. Most evidence pointed out that the failure resulted from corrosion attack due to condensation of hydrochloric acid. Misalignment of the pipe at the flange led to cold work which is also thought to accelerate the corrosion rate. It was recommended to consider a better pipe alignment practice as well as the addition of an inhibitor as a short-term solution. Since the piping system was used close to the critical operating conditions. it was recommended as a long-term solution to replace the caustic header material by one of the higher grades Ni-Cr-Mo alloys.
eu_rights_str_mv openAccess
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identifier_str_mv Corrosion of carbon steel caustic header in the presence of chloride ions. Engineering Failure Analysis.
language_invalid_str_mv en
network_acronym_str KFUPM
network_name_str King Fahd University of Petroleum and Minerals
oai_identifier_str oai::136056
publishDate 2020
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spelling Corrosion of carbon steel caustic header in the presence of chloride ionsUl-Hamid, AnwarunknownCorrosionCaustic soda produced in caustic cells at a petrochemical plant was loaded into a crude tank by means of a caustic header line made of plain carbon steel. After a fraction of expected service life, the header was severely corroded. Scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDS) and X-ray diffraction (XRD) was used to identify the material and the corrosion product. Metallurgical evaluation suggested that the mode of failure was localized attack by chlorine and/or hydrochloric acid at pipe connections (flanges) where concentrated solutions could accumulate. Most evidence pointed out that the failure resulted from corrosion attack due to condensation of hydrochloric acid. Misalignment of the pipe at the flange led to cold work which is also thought to accelerate the corrosion rate. It was recommended to consider a better pipe alignment practice as well as the addition of an inhibitor as a short-term solution. Since the piping system was used close to the critical operating conditions. it was recommended as a long-term solution to replace the caustic header material by one of the higher grades Ni-Cr-Mo alloys.ArticlePeerReviewedinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttps://eprints.kfupm.edu.sa/id/eprint/136056/1/anwar_Corrosion_carbon_steel_caustic_header_the_presence_of_chloride_ions.pdf Corrosion of carbon steel caustic header in the presence of chloride ions. Engineering Failure Analysis. enhttps://eprints.kfupm.edu.sa/id/eprint/136056/2020info:eu-repo/semantics/openAccessoai::1360562021-08-01T11:45:20Z
spellingShingle Corrosion of carbon steel caustic header in the presence of chloride ions
Ul-Hamid, Anwar
Corrosion
status_str publishedVersion
title Corrosion of carbon steel caustic header in the presence of chloride ions
title_full Corrosion of carbon steel caustic header in the presence of chloride ions
title_fullStr Corrosion of carbon steel caustic header in the presence of chloride ions
title_full_unstemmed Corrosion of carbon steel caustic header in the presence of chloride ions
title_short Corrosion of carbon steel caustic header in the presence of chloride ions
title_sort Corrosion of carbon steel caustic header in the presence of chloride ions
topic Corrosion
url https://eprints.kfupm.edu.sa/id/eprint/136056/1/anwar_Corrosion_carbon_steel_caustic_header_the_presence_of_chloride_ions.pdf