Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries

<p dir="ltr">In this work, phase pure and highly crystalline O3-type layered oxide material (Na<sub>1</sub>Ni<sub>0.33</sub>Mn<sub>0.33</sub>Fe<sub>0.33</sub>O<sub>2</sub>-NNMF) was developed using; (i) a conventional solid-...

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التفاصيل البيبلوغرافية
المؤلف الرئيسي: R.A. Harindi Gayara (17821406) (author)
مؤلفون آخرون: Buzaina Moossa (17337883) (author), R.A. Shakoor (17017692) (author), Rana Faisal Shahzad (17746935) (author), Muhammad Sajjad (722125) (author), Nirpendra Singh (414952) (author), Shahid Rasul (5146139) (author), Talal Mohammed Al tahtamouni (17280763) (author)
منشور في: 2023
الموضوعات:
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author R.A. Harindi Gayara (17821406)
author2 Buzaina Moossa (17337883)
R.A. Shakoor (17017692)
Rana Faisal Shahzad (17746935)
Muhammad Sajjad (722125)
Nirpendra Singh (414952)
Shahid Rasul (5146139)
Talal Mohammed Al tahtamouni (17280763)
author2_role author
author
author
author
author
author
author
author_facet R.A. Harindi Gayara (17821406)
Buzaina Moossa (17337883)
R.A. Shakoor (17017692)
Rana Faisal Shahzad (17746935)
Muhammad Sajjad (722125)
Nirpendra Singh (414952)
Shahid Rasul (5146139)
Talal Mohammed Al tahtamouni (17280763)
author_role author
dc.creator.none.fl_str_mv R.A. Harindi Gayara (17821406)
Buzaina Moossa (17337883)
R.A. Shakoor (17017692)
Rana Faisal Shahzad (17746935)
Muhammad Sajjad (722125)
Nirpendra Singh (414952)
Shahid Rasul (5146139)
Talal Mohammed Al tahtamouni (17280763)
dc.date.none.fl_str_mv 2023-11-01T00:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.egyr.2023.07.038
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Cost-effective_microwave-assisted_O3-_type_sodium-based_layered_oxide_cathode_materials_for_sodium-ion_batteries/25036721
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Engineering
Chemical engineering
Electrical engineering
Materials engineering
Sol–gel
O3-type layered oxide
Cathode materials
Sodium-ion battery
Energy storage
dc.title.none.fl_str_mv Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">In this work, phase pure and highly crystalline O3-type layered oxide material (Na<sub>1</sub>Ni<sub>0.33</sub>Mn<sub>0.33</sub>Fe<sub>0.33</sub>O<sub>2</sub>-NNMF) was developed using; (i) a conventional solid-state synthesis route and (ii) a facile microwave-assisted sol–gel technique. A comparison of structural, thermal, and electrochemical properties is presented to elucidate the usefulness of the microwave-assisted sol–gel synthesis technique. A remarkable reduction in the sintering process time is noticed in the microwave-assisted sol–gel synthesis technique without compromising on the structural, thermal and electrochemical properties when compared to the conventional solid-state synthesis route confirming its decent cost-effectiveness. It is further noticed that NNMF developed through microwave-assisted sol–gel synthesis technique demonstrates superior thermal stability and comparable electrochemical performance as compared to the same material produced through the conventional sintering process. The decent electrochemical properties induced in NNMF during the microwave-assisted sol–gel synthesis technique can be attributed to the efficient diffusion of Na <sup>+</sup> ions into/from the host structure during the intercalation/de-intercalation process as indicated by the high value of sodium diffusion coefficient (1 × 10<sup>9</sup>-3.58 × 10<sup>9</sup> m<sup>2</sup> s<sup>− 1</sup>). The Potentiostatic Intermittent Titration Technique (PITT) analysis confirms single-phase Na + intercalation/deintercalation in the host structure, regardless of the synthesis process. Finally, EIS analysis confirms the capacity fading of the developed materials during the cycling process is essentially due to an increase in the resistance with the increasing number of cycles due to the gradual thickening of formed SEI layer. The microwave-assisted sol–gel synthesis technique can be effectively employed for the production of many families of cathode materials at competitive cost facilitating their commercialization.</p><h2>Other Information</h2><p dir="ltr">Published in: Energy Reports<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.egyr.2023.07.038" target="_blank">https://dx.doi.org/10.1016/j.egyr.2023.07.038</a></p>
eu_rights_str_mv openAccess
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network_acronym_str Manara2
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oai_identifier_str oai:figshare.com:article/25036721
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spelling Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteriesR.A. Harindi Gayara (17821406)Buzaina Moossa (17337883)R.A. Shakoor (17017692)Rana Faisal Shahzad (17746935)Muhammad Sajjad (722125)Nirpendra Singh (414952)Shahid Rasul (5146139)Talal Mohammed Al tahtamouni (17280763)EngineeringChemical engineeringElectrical engineeringMaterials engineeringSol–gelO3-type layered oxideCathode materialsSodium-ion batteryEnergy storage<p dir="ltr">In this work, phase pure and highly crystalline O3-type layered oxide material (Na<sub>1</sub>Ni<sub>0.33</sub>Mn<sub>0.33</sub>Fe<sub>0.33</sub>O<sub>2</sub>-NNMF) was developed using; (i) a conventional solid-state synthesis route and (ii) a facile microwave-assisted sol–gel technique. A comparison of structural, thermal, and electrochemical properties is presented to elucidate the usefulness of the microwave-assisted sol–gel synthesis technique. A remarkable reduction in the sintering process time is noticed in the microwave-assisted sol–gel synthesis technique without compromising on the structural, thermal and electrochemical properties when compared to the conventional solid-state synthesis route confirming its decent cost-effectiveness. It is further noticed that NNMF developed through microwave-assisted sol–gel synthesis technique demonstrates superior thermal stability and comparable electrochemical performance as compared to the same material produced through the conventional sintering process. The decent electrochemical properties induced in NNMF during the microwave-assisted sol–gel synthesis technique can be attributed to the efficient diffusion of Na <sup>+</sup> ions into/from the host structure during the intercalation/de-intercalation process as indicated by the high value of sodium diffusion coefficient (1 × 10<sup>9</sup>-3.58 × 10<sup>9</sup> m<sup>2</sup> s<sup>− 1</sup>). The Potentiostatic Intermittent Titration Technique (PITT) analysis confirms single-phase Na + intercalation/deintercalation in the host structure, regardless of the synthesis process. Finally, EIS analysis confirms the capacity fading of the developed materials during the cycling process is essentially due to an increase in the resistance with the increasing number of cycles due to the gradual thickening of formed SEI layer. The microwave-assisted sol–gel synthesis technique can be effectively employed for the production of many families of cathode materials at competitive cost facilitating their commercialization.</p><h2>Other Information</h2><p dir="ltr">Published in: Energy Reports<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.egyr.2023.07.038" target="_blank">https://dx.doi.org/10.1016/j.egyr.2023.07.038</a></p>2023-11-01T00:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.egyr.2023.07.038https://figshare.com/articles/journal_contribution/Cost-effective_microwave-assisted_O3-_type_sodium-based_layered_oxide_cathode_materials_for_sodium-ion_batteries/25036721CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/250367212023-11-01T00:00:00Z
spellingShingle Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries
R.A. Harindi Gayara (17821406)
Engineering
Chemical engineering
Electrical engineering
Materials engineering
Sol–gel
O3-type layered oxide
Cathode materials
Sodium-ion battery
Energy storage
status_str publishedVersion
title Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries
title_full Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries
title_fullStr Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries
title_full_unstemmed Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries
title_short Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries
title_sort Cost-effective microwave-assisted O3- type sodium-based layered oxide cathode materials for sodium-ion batteries
topic Engineering
Chemical engineering
Electrical engineering
Materials engineering
Sol–gel
O3-type layered oxide
Cathode materials
Sodium-ion battery
Energy storage