Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark

<p dir="ltr">Nanomaterial such as metals and metal oxide photocatalysts have emerged as important tools for removing contaminants from wastewater and as antibacterial agents to prevent infections; this is mainly due to their stability under different irradiation conditions. Herein, t...

وصف كامل

محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Maha Matalkeh (17148358) (author)
مؤلفون آخرون: Gheyath K. Nasrallah (9200525) (author), Farah M. Shurrab (16324961) (author), Enas S. Al-Absi (6281936) (author), Widad Mohammed (17148361) (author), Ahmed Elzatahry (1515655) (author), Khaled M. Saoud (16876017) (author)
منشور في: 2022
الموضوعات:
الوسوم: إضافة وسم
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author Maha Matalkeh (17148358)
author2 Gheyath K. Nasrallah (9200525)
Farah M. Shurrab (16324961)
Enas S. Al-Absi (6281936)
Widad Mohammed (17148361)
Ahmed Elzatahry (1515655)
Khaled M. Saoud (16876017)
author2_role author
author
author
author
author
author
author_facet Maha Matalkeh (17148358)
Gheyath K. Nasrallah (9200525)
Farah M. Shurrab (16324961)
Enas S. Al-Absi (6281936)
Widad Mohammed (17148361)
Ahmed Elzatahry (1515655)
Khaled M. Saoud (16876017)
author_role author
dc.creator.none.fl_str_mv Maha Matalkeh (17148358)
Gheyath K. Nasrallah (9200525)
Farah M. Shurrab (16324961)
Enas S. Al-Absi (6281936)
Widad Mohammed (17148361)
Ahmed Elzatahry (1515655)
Khaled M. Saoud (16876017)
dc.date.none.fl_str_mv 2022-03-01T00:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.rineng.2021.100313
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Visible_Light_Photocatalytic_Activity_of_Ag_WO_sub_3_sub_Nanoparticles_and_its_Antibacterial_Activity_Under_Ambient_Light_and_in_The_Dark/24311869
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Engineering
Electronics, sensors and digital hardware
Nanotechnology
Visible Light
Photocatalytic
Ag/WO3 Nanoparticles
Ambient Light
dc.title.none.fl_str_mv Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">Nanomaterial such as metals and metal oxide photocatalysts have emerged as important tools for removing contaminants from wastewater and as antibacterial agents to prevent infections; this is mainly due to their stability under different irradiation conditions. Herein, the catalytic and antimicrobial activities of nanocrystalline silver (Ag), supported on tungsten oxide (WO<sub>3</sub>) nanoparticles prepared using the deposition-precipitation synthesis technique, are studied. The synthesized material was characterized as XRD, XPS, TEM, and TEM-EDS to investigate their physio-chemical properties. HRTEM, XPS analysis shows that the photocatalyst has a large sheet-like morphology with well-dispersed small metallic Ag particles (<3 nm) on the WO<sub>3</sub> nanoparticle's surface, with most particles near the edges. Ultraviolet–visible spectra analysis observed a large redshift in the absorbing band edge and decreased bandgap energy from 2.6 to 2.1 eV. Photocatalytic analysis at different concentrations of 1% Ag/WO<sub>3</sub> under visible light indicated a high degradation efficiency. The largest degradation efficiency of Methylene Blue (MB) under visible light irradiation was (∼80%) in 120 min at 1 g/L catalyst dosage. The photodegradation of MB under visible light as a function of catalyst dose followed the pseudo-first-order kinetics. In addition, the catalyst shows high degradation efficiency and significant dose-dependent inhibition of Gram-negative E. Coli and the Gram-positive S. aureus. Furthermore, the catalyst showed excellent stability and recyclability.</p><h2>Other Information</h2><p dir="ltr">Published in: Results in Engineering<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.rineng.2021.100313" target="_blank">https://dx.doi.org/10.1016/j.rineng.2021.100313</a></p><p dir="ltr">Additional institutions affiliated with: Liberal Arts and Science - VCUarts Qatar</p>
eu_rights_str_mv openAccess
id Manara2_08338c981067012103b0e322c3acb8fb
identifier_str_mv 10.1016/j.rineng.2021.100313
network_acronym_str Manara2
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oai_identifier_str oai:figshare.com:article/24311869
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spelling Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The DarkMaha Matalkeh (17148358)Gheyath K. Nasrallah (9200525)Farah M. Shurrab (16324961)Enas S. Al-Absi (6281936)Widad Mohammed (17148361)Ahmed Elzatahry (1515655)Khaled M. Saoud (16876017)EngineeringElectronics, sensors and digital hardwareNanotechnologyVisible LightPhotocatalyticAg/WO3 NanoparticlesAmbient Light<p dir="ltr">Nanomaterial such as metals and metal oxide photocatalysts have emerged as important tools for removing contaminants from wastewater and as antibacterial agents to prevent infections; this is mainly due to their stability under different irradiation conditions. Herein, the catalytic and antimicrobial activities of nanocrystalline silver (Ag), supported on tungsten oxide (WO<sub>3</sub>) nanoparticles prepared using the deposition-precipitation synthesis technique, are studied. The synthesized material was characterized as XRD, XPS, TEM, and TEM-EDS to investigate their physio-chemical properties. HRTEM, XPS analysis shows that the photocatalyst has a large sheet-like morphology with well-dispersed small metallic Ag particles (<3 nm) on the WO<sub>3</sub> nanoparticle's surface, with most particles near the edges. Ultraviolet–visible spectra analysis observed a large redshift in the absorbing band edge and decreased bandgap energy from 2.6 to 2.1 eV. Photocatalytic analysis at different concentrations of 1% Ag/WO<sub>3</sub> under visible light indicated a high degradation efficiency. The largest degradation efficiency of Methylene Blue (MB) under visible light irradiation was (∼80%) in 120 min at 1 g/L catalyst dosage. The photodegradation of MB under visible light as a function of catalyst dose followed the pseudo-first-order kinetics. In addition, the catalyst shows high degradation efficiency and significant dose-dependent inhibition of Gram-negative E. Coli and the Gram-positive S. aureus. Furthermore, the catalyst showed excellent stability and recyclability.</p><h2>Other Information</h2><p dir="ltr">Published in: Results in Engineering<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.rineng.2021.100313" target="_blank">https://dx.doi.org/10.1016/j.rineng.2021.100313</a></p><p dir="ltr">Additional institutions affiliated with: Liberal Arts and Science - VCUarts Qatar</p>2022-03-01T00:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.rineng.2021.100313https://figshare.com/articles/journal_contribution/Visible_Light_Photocatalytic_Activity_of_Ag_WO_sub_3_sub_Nanoparticles_and_its_Antibacterial_Activity_Under_Ambient_Light_and_in_The_Dark/24311869CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/243118692022-03-01T00:00:00Z
spellingShingle Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark
Maha Matalkeh (17148358)
Engineering
Electronics, sensors and digital hardware
Nanotechnology
Visible Light
Photocatalytic
Ag/WO3 Nanoparticles
Ambient Light
status_str publishedVersion
title Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark
title_full Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark
title_fullStr Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark
title_full_unstemmed Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark
title_short Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark
title_sort Visible Light Photocatalytic Activity of Ag/WO<sub>3</sub> Nanoparticles and its Antibacterial Activity Under Ambient Light and in The Dark
topic Engineering
Electronics, sensors and digital hardware
Nanotechnology
Visible Light
Photocatalytic
Ag/WO3 Nanoparticles
Ambient Light