Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals

<div><p>The remarkable adsorption capacity of graphene-derived materials has prompted their examination in composite materials suitable for deployment in treatment of contaminated waters. In this study, crosslinked calcium alginate–graphene oxide beads were prepared and activated by expo...

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محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Burcu Gunes (18527739) (author)
مؤلفون آخرون: Yannick Jaquet (18527742) (author), Laura Sánchez (471954) (author), Rebecca Pumarino (18527745) (author), Declan McGlade (18527748) (author), Brid Quilty (1976071) (author), Anne Morrissey (292738) (author), Zahra Gholamvand (1423744) (author), Kieran Nolan (2047333) (author), Jenny Lawler (16931817) (author)
منشور في: 2021
الموضوعات:
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author Burcu Gunes (18527739)
author2 Yannick Jaquet (18527742)
Laura Sánchez (471954)
Rebecca Pumarino (18527745)
Declan McGlade (18527748)
Brid Quilty (1976071)
Anne Morrissey (292738)
Zahra Gholamvand (1423744)
Kieran Nolan (2047333)
Jenny Lawler (16931817)
author2_role author
author
author
author
author
author
author
author
author
author_facet Burcu Gunes (18527739)
Yannick Jaquet (18527742)
Laura Sánchez (471954)
Rebecca Pumarino (18527745)
Declan McGlade (18527748)
Brid Quilty (1976071)
Anne Morrissey (292738)
Zahra Gholamvand (1423744)
Kieran Nolan (2047333)
Jenny Lawler (16931817)
author_role author
dc.creator.none.fl_str_mv Burcu Gunes (18527739)
Yannick Jaquet (18527742)
Laura Sánchez (471954)
Rebecca Pumarino (18527745)
Declan McGlade (18527748)
Brid Quilty (1976071)
Anne Morrissey (292738)
Zahra Gholamvand (1423744)
Kieran Nolan (2047333)
Jenny Lawler (16931817)
dc.date.none.fl_str_mv 2021-10-23T03:00:00Z
dc.identifier.none.fl_str_mv 10.3390/ma14216343
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Activated_Graphene_Oxide-Calcium_Alginate_Beads_for_Adsorption_of_Methylene_Blue_and_Pharmaceuticals/25780980
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Engineering
Environmental engineering
Environmental sciences
Environmental management
adsorption
graphene oxide
methylene blue
pharmaceuticals
kinetics
isotherms and thermodynamics
dc.title.none.fl_str_mv Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <div><p>The remarkable adsorption capacity of graphene-derived materials has prompted their examination in composite materials suitable for deployment in treatment of contaminated waters. In this study, crosslinked calcium alginate–graphene oxide beads were prepared and activated by exposure to pH 4 by using 0.1M HCl. The activated beads were investigated as novel adsorbents for the removal of organic pollutants (methylene blue dye and the pharmaceuticals famotidine and diclofenac) with a range of physicochemical properties. The effects of initial pollutant concentration, temperature, pH, and adsorbent dose were investigated, and kinetic models were examined for fit to the data. The maximum adsorption capacities qmax obtained were 1334, 35.50 and 36.35 mg g−1 for the uptake of methylene blue, famotidine and diclofenac, respectively. The equilibrium adsorption had an alignment with Langmuir isotherms, while the kinetics were most accurately modelled using pseudo- first-order and second order models according to the regression analysis. Thermodynamic parameters such as ΔG°, ΔH° and ΔS° were calculated and the adsorption process was determined to be exothermic and spontaneous.</p><p> </p></div><h2>Other Information</h2> <p> Published in: Materials<br> License: <a href="https://creativecommons.org/licenses/by/4.0/" target="_blank">https://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.3390/ma14216343" target="_blank">https://dx.doi.org/10.3390/ma14216343</a></p>
eu_rights_str_mv openAccess
id Manara2_0d712c29db90b9065b6fb7286ae782b2
identifier_str_mv 10.3390/ma14216343
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/25780980
publishDate 2021
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rights_invalid_str_mv CC BY 4.0
spelling Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and PharmaceuticalsBurcu Gunes (18527739)Yannick Jaquet (18527742)Laura Sánchez (471954)Rebecca Pumarino (18527745)Declan McGlade (18527748)Brid Quilty (1976071)Anne Morrissey (292738)Zahra Gholamvand (1423744)Kieran Nolan (2047333)Jenny Lawler (16931817)EngineeringEnvironmental engineeringEnvironmental sciencesEnvironmental managementadsorptiongraphene oxidemethylene bluepharmaceuticalskineticsisotherms and thermodynamics<div><p>The remarkable adsorption capacity of graphene-derived materials has prompted their examination in composite materials suitable for deployment in treatment of contaminated waters. In this study, crosslinked calcium alginate–graphene oxide beads were prepared and activated by exposure to pH 4 by using 0.1M HCl. The activated beads were investigated as novel adsorbents for the removal of organic pollutants (methylene blue dye and the pharmaceuticals famotidine and diclofenac) with a range of physicochemical properties. The effects of initial pollutant concentration, temperature, pH, and adsorbent dose were investigated, and kinetic models were examined for fit to the data. The maximum adsorption capacities qmax obtained were 1334, 35.50 and 36.35 mg g−1 for the uptake of methylene blue, famotidine and diclofenac, respectively. The equilibrium adsorption had an alignment with Langmuir isotherms, while the kinetics were most accurately modelled using pseudo- first-order and second order models according to the regression analysis. Thermodynamic parameters such as ΔG°, ΔH° and ΔS° were calculated and the adsorption process was determined to be exothermic and spontaneous.</p><p> </p></div><h2>Other Information</h2> <p> Published in: Materials<br> License: <a href="https://creativecommons.org/licenses/by/4.0/" target="_blank">https://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.3390/ma14216343" target="_blank">https://dx.doi.org/10.3390/ma14216343</a></p>2021-10-23T03:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.3390/ma14216343https://figshare.com/articles/journal_contribution/Activated_Graphene_Oxide-Calcium_Alginate_Beads_for_Adsorption_of_Methylene_Blue_and_Pharmaceuticals/25780980CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/257809802021-10-23T03:00:00Z
spellingShingle Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals
Burcu Gunes (18527739)
Engineering
Environmental engineering
Environmental sciences
Environmental management
adsorption
graphene oxide
methylene blue
pharmaceuticals
kinetics
isotherms and thermodynamics
status_str publishedVersion
title Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals
title_full Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals
title_fullStr Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals
title_full_unstemmed Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals
title_short Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals
title_sort Activated Graphene Oxide-Calcium Alginate Beads for Adsorption of Methylene Blue and Pharmaceuticals
topic Engineering
Environmental engineering
Environmental sciences
Environmental management
adsorption
graphene oxide
methylene blue
pharmaceuticals
kinetics
isotherms and thermodynamics