Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology
<p>To control Fe3O4 nanoparticles (Fe3O4 NPs) size, different molar ratio of Fe2+ and Fe3+ as well as ammonium hydroxide (pH) was used to synthesize Fe3O4 NPs through co-precipitation method. The Box–Behnken design was selected to explore the interaction between process parameters (factors) su...
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| مؤلفون آخرون: | , , , , |
| منشور في: |
2022
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| _version_ | 1864513567215058944 |
|---|---|
| author | Muneer M. Ba-Abbad (14151660) |
| author2 | P. V. Chai (14151888) Abdelbaki Benamour (14151891) Dina Ewis (14149998) Abdul Wahab Mohammad (1732102) Ebrahim Mahmoudi (14151894) |
| author2_role | author author author author author |
| author_facet | Muneer M. Ba-Abbad (14151660) P. V. Chai (14151888) Abdelbaki Benamour (14151891) Dina Ewis (14149998) Abdul Wahab Mohammad (1732102) Ebrahim Mahmoudi (14151894) |
| author_role | author |
| dc.creator.none.fl_str_mv | Muneer M. Ba-Abbad (14151660) P. V. Chai (14151888) Abdelbaki Benamour (14151891) Dina Ewis (14149998) Abdul Wahab Mohammad (1732102) Ebrahim Mahmoudi (14151894) |
| dc.date.none.fl_str_mv | 2022-11-22T21:14:57Z |
| dc.identifier.none.fl_str_mv | 10.1007/s11696-022-02320-y |
| dc.relation.none.fl_str_mv | https://figshare.com/articles/journal_contribution/Optimizing_and_control_of_effective_synthesize_parameters_for_Fe3O4_nanoparticles_using_response_surface_methodology/21597630 |
| dc.rights.none.fl_str_mv | CC BY 4.0 info:eu-repo/semantics/openAccess |
| dc.subject.none.fl_str_mv | Macromolecular and materials chemistry Manufacturing engineering Materials Chemistry Industrial and Manufacturing Engineering General Chemical Engineering Biochemistry General Chemistry |
| dc.title.none.fl_str_mv | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology |
| dc.type.none.fl_str_mv | Text Journal contribution info:eu-repo/semantics/publishedVersion text contribution to journal |
| description | <p>To control Fe3O4 nanoparticles (Fe3O4 NPs) size, different molar ratio of Fe2+ and Fe3+ as well as ammonium hydroxide (pH) was used to synthesize Fe3O4 NPs through co-precipitation method. The Box–Behnken design was selected to explore the interaction between process parameters (factors) such as Fe2+ molar ion, Fe3+ molar ion and pH on the final size. The interactive effect between the process variables was evaluated by analysis of variance (ANOVA). The quadratic model predicted by the Box–Behnken design was significant with a P value of < 0.0001. The optimum synthesis conditions were predicted by the model indicating optimum size obtained using 1.00 mol Fe2+ ion with 3.00 mol Fe3+ ion with pH at 12.00. From the experiment, the particle size was 10 ± 2 nm at optimum conditions, while the model predicted a particle size of 6.80 nm. The magnetic properties of Fe3O4 NPs were displayed typical ferromagnetic behavior with saturation magnetization value to be 49.729 emu/g. Finally, the optimized Fe3O4 NPs showed about 80% removal of Congo red (CR) dye, which confirms their applicability in adsorption process for future applications.</p><h2>Other Information</h2> <p> Published in: Chemical Papers<br> License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="http://dx.doi.org/10.1007/s11696-022-02320-y" target="_blank">http://dx.doi.org/10.1007/s11696-022-02320-y</a></p> |
| eu_rights_str_mv | openAccess |
| id | Manara2_10971393dc3663dd9215780322eca4b8 |
| identifier_str_mv | 10.1007/s11696-022-02320-y |
| network_acronym_str | Manara2 |
| network_name_str | Manara2 |
| oai_identifier_str | oai:figshare.com:article/21597630 |
| publishDate | 2022 |
| repository.mail.fl_str_mv | |
| repository.name.fl_str_mv | |
| repository_id_str | |
| rights_invalid_str_mv | CC BY 4.0 |
| spelling | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodologyMuneer M. Ba-Abbad (14151660)P. V. Chai (14151888)Abdelbaki Benamour (14151891)Dina Ewis (14149998)Abdul Wahab Mohammad (1732102)Ebrahim Mahmoudi (14151894)Macromolecular and materials chemistryManufacturing engineeringMaterials ChemistryIndustrial and Manufacturing EngineeringGeneral Chemical EngineeringBiochemistryGeneral Chemistry<p>To control Fe3O4 nanoparticles (Fe3O4 NPs) size, different molar ratio of Fe2+ and Fe3+ as well as ammonium hydroxide (pH) was used to synthesize Fe3O4 NPs through co-precipitation method. The Box–Behnken design was selected to explore the interaction between process parameters (factors) such as Fe2+ molar ion, Fe3+ molar ion and pH on the final size. The interactive effect between the process variables was evaluated by analysis of variance (ANOVA). The quadratic model predicted by the Box–Behnken design was significant with a P value of < 0.0001. The optimum synthesis conditions were predicted by the model indicating optimum size obtained using 1.00 mol Fe2+ ion with 3.00 mol Fe3+ ion with pH at 12.00. From the experiment, the particle size was 10 ± 2 nm at optimum conditions, while the model predicted a particle size of 6.80 nm. The magnetic properties of Fe3O4 NPs were displayed typical ferromagnetic behavior with saturation magnetization value to be 49.729 emu/g. Finally, the optimized Fe3O4 NPs showed about 80% removal of Congo red (CR) dye, which confirms their applicability in adsorption process for future applications.</p><h2>Other Information</h2> <p> Published in: Chemical Papers<br> License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="http://dx.doi.org/10.1007/s11696-022-02320-y" target="_blank">http://dx.doi.org/10.1007/s11696-022-02320-y</a></p>2022-11-22T21:14:57ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1007/s11696-022-02320-yhttps://figshare.com/articles/journal_contribution/Optimizing_and_control_of_effective_synthesize_parameters_for_Fe3O4_nanoparticles_using_response_surface_methodology/21597630CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/215976302022-11-22T21:14:57Z |
| spellingShingle | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology Muneer M. Ba-Abbad (14151660) Macromolecular and materials chemistry Manufacturing engineering Materials Chemistry Industrial and Manufacturing Engineering General Chemical Engineering Biochemistry General Chemistry |
| status_str | publishedVersion |
| title | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology |
| title_full | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology |
| title_fullStr | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology |
| title_full_unstemmed | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology |
| title_short | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology |
| title_sort | Optimizing and control of effective synthesize parameters for Fe3O4 nanoparticles using response surface methodology |
| topic | Macromolecular and materials chemistry Manufacturing engineering Materials Chemistry Industrial and Manufacturing Engineering General Chemical Engineering Biochemistry General Chemistry |