Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels

<p>The effect of cementite morphology on the crack initiation and growth path was studied using in situ electrochem-ical micro-cantilever bending (ECCB) technique under hydrogen (H) charging. Two carbon steels with lamellar cementite morphology (pearlitic microstructure) and spherical or broke...

وصف كامل

محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Shabnam Karimi (19457575) (author)
مؤلفون آخرون: Iman Taji (19457578) (author), Tarlan Hajilou (19457587) (author), Afrooz Barnoush (7410176) (author), Roy Johnsen (19457590) (author)
منشور في: 2022
الموضوعات:
الوسوم: إضافة وسم
لا توجد وسوم, كن أول من يضع وسما على هذه التسجيلة!
_version_ 1864513506620997632
author Shabnam Karimi (19457575)
author2 Iman Taji (19457578)
Tarlan Hajilou (19457587)
Afrooz Barnoush (7410176)
Roy Johnsen (19457590)
author2_role author
author
author
author
author_facet Shabnam Karimi (19457575)
Iman Taji (19457578)
Tarlan Hajilou (19457587)
Afrooz Barnoush (7410176)
Roy Johnsen (19457590)
author_role author
dc.creator.none.fl_str_mv Shabnam Karimi (19457575)
Iman Taji (19457578)
Tarlan Hajilou (19457587)
Afrooz Barnoush (7410176)
Roy Johnsen (19457590)
dc.date.none.fl_str_mv 2022-03-28T12:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.ijhydene.2022.01.222
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Evaluation_of_the_cementite_morphology_influence_on_the_hydrogen_induced_crack_nucleation_and_propagation_path_in_carbon_steels/26862472
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Physical chemistry
Engineering
Materials engineering
Hydrogen embrittlement
Carbon steels
Cementite
Spheroidite
Pearlite
Micro-cantilever
dc.title.none.fl_str_mv Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p>The effect of cementite morphology on the crack initiation and growth path was studied using in situ electrochem-ical micro-cantilever bending (ECCB) technique under hydrogen (H) charging. Two carbon steels with lamellar cementite morphology (pearlitic microstructure) and spherical or broken lamellas cementite morphology (spheroidite microstructure), both with approximately the same carbon equivalent, were used in this study. The ECCB tests were performed in H-free and two H charging steps with −1050 mV and −1550 mV charging potential versus Ag/AgCl reference electrode. The results show that both materials are resistant to crack initiation in the H-free condition while under −1050 mV charging, crack propagates through the grain boundaries in a tortuous path in spheroidite mi-crostructure and the lamellar microstructure displayed a higher strength with small cracks propagating through both the grain boundaries and the lamellas. A drastic load decrease in the load-displacement (L-D) curve happened under −1550 mV charging for both microstructures accompanied by a straight crack growth path in spheroidite microstruc-ture, independent of grain boundaries or ferrite-cementite interfaces while a competition between the shear crack growth mechanism and the interfacial cracking determines the crack growth path in the lamellar microstructure.</p><h2>Other Information</h2> <p> Published in: International Journal of Hydrogen Energy<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.ijhydene.2022.01.222" target="_blank">https://dx.doi.org/10.1016/j.ijhydene.2022.01.222</a></p>
eu_rights_str_mv openAccess
id Manara2_130b44180d7c32e707d1c60ee0458762
identifier_str_mv 10.1016/j.ijhydene.2022.01.222
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/26862472
publishDate 2022
repository.mail.fl_str_mv
repository.name.fl_str_mv
repository_id_str
rights_invalid_str_mv CC BY 4.0
spelling Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steelsShabnam Karimi (19457575)Iman Taji (19457578)Tarlan Hajilou (19457587)Afrooz Barnoush (7410176)Roy Johnsen (19457590)Chemical sciencesPhysical chemistryEngineeringMaterials engineeringHydrogen embrittlementCarbon steelsCementiteSpheroiditePearliteMicro-cantilever<p>The effect of cementite morphology on the crack initiation and growth path was studied using in situ electrochem-ical micro-cantilever bending (ECCB) technique under hydrogen (H) charging. Two carbon steels with lamellar cementite morphology (pearlitic microstructure) and spherical or broken lamellas cementite morphology (spheroidite microstructure), both with approximately the same carbon equivalent, were used in this study. The ECCB tests were performed in H-free and two H charging steps with −1050 mV and −1550 mV charging potential versus Ag/AgCl reference electrode. The results show that both materials are resistant to crack initiation in the H-free condition while under −1050 mV charging, crack propagates through the grain boundaries in a tortuous path in spheroidite mi-crostructure and the lamellar microstructure displayed a higher strength with small cracks propagating through both the grain boundaries and the lamellas. A drastic load decrease in the load-displacement (L-D) curve happened under −1550 mV charging for both microstructures accompanied by a straight crack growth path in spheroidite microstruc-ture, independent of grain boundaries or ferrite-cementite interfaces while a competition between the shear crack growth mechanism and the interfacial cracking determines the crack growth path in the lamellar microstructure.</p><h2>Other Information</h2> <p> Published in: International Journal of Hydrogen Energy<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.ijhydene.2022.01.222" target="_blank">https://dx.doi.org/10.1016/j.ijhydene.2022.01.222</a></p>2022-03-28T12:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.ijhydene.2022.01.222https://figshare.com/articles/journal_contribution/Evaluation_of_the_cementite_morphology_influence_on_the_hydrogen_induced_crack_nucleation_and_propagation_path_in_carbon_steels/26862472CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/268624722022-03-28T12:00:00Z
spellingShingle Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels
Shabnam Karimi (19457575)
Chemical sciences
Physical chemistry
Engineering
Materials engineering
Hydrogen embrittlement
Carbon steels
Cementite
Spheroidite
Pearlite
Micro-cantilever
status_str publishedVersion
title Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels
title_full Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels
title_fullStr Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels
title_full_unstemmed Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels
title_short Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels
title_sort Evaluation of the cementite morphology influence on the hydrogen induced crack nucleation and propagation path in carbon steels
topic Chemical sciences
Physical chemistry
Engineering
Materials engineering
Hydrogen embrittlement
Carbon steels
Cementite
Spheroidite
Pearlite
Micro-cantilever