Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications

<p dir="ltr">Aloe vera (Aloe barbadensis miller) leaf extract was used in green fuel-assisted microwave synthesis to prepare Calcium Magnesium Aluminate (CMA). The synthesized CMA was characterized by X-ray diffraction (XRD), Fourier transform-infrared (FT-IR), Scanning electron micr...

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Main Author: H.V. Harini (22224871) (author)
Other Authors: H.P. Nagaswarupa (22224874) (author), Ramachandra Naik (22224877) (author), L. Guddi Likmaram (22224880) (author), S.K. Sukrutha (22224883) (author), S.N. Pramod (22224886) (author), Ramyakrishna Pothu (17792591) (author), Mika Sillanpää (765189) (author), Rajender Boddula (4636810) (author), Ahmed Bahgat Radwan (17380297) (author), Noora Al-Qahtani (15314043) (author)
Published: 2024
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author H.V. Harini (22224871)
author2 H.P. Nagaswarupa (22224874)
Ramachandra Naik (22224877)
L. Guddi Likmaram (22224880)
S.K. Sukrutha (22224883)
S.N. Pramod (22224886)
Ramyakrishna Pothu (17792591)
Mika Sillanpää (765189)
Rajender Boddula (4636810)
Ahmed Bahgat Radwan (17380297)
Noora Al-Qahtani (15314043)
author2_role author
author
author
author
author
author
author
author
author
author
author_facet H.V. Harini (22224871)
H.P. Nagaswarupa (22224874)
Ramachandra Naik (22224877)
L. Guddi Likmaram (22224880)
S.K. Sukrutha (22224883)
S.N. Pramod (22224886)
Ramyakrishna Pothu (17792591)
Mika Sillanpää (765189)
Rajender Boddula (4636810)
Ahmed Bahgat Radwan (17380297)
Noora Al-Qahtani (15314043)
author_role author
dc.creator.none.fl_str_mv H.V. Harini (22224871)
H.P. Nagaswarupa (22224874)
Ramachandra Naik (22224877)
L. Guddi Likmaram (22224880)
S.K. Sukrutha (22224883)
S.N. Pramod (22224886)
Ramyakrishna Pothu (17792591)
Mika Sillanpää (765189)
Rajender Boddula (4636810)
Ahmed Bahgat Radwan (17380297)
Noora Al-Qahtani (15314043)
dc.date.none.fl_str_mv 2024-09-27T15:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.inoche.2024.113185
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Bioinspired_synthesis_of_calcium_magnesium_aluminate_nanoparticles_using_aloe_vera_extract_A_promising_material_for_electrochemical_sensors_antibacterial_and_environmental_remediation_applications/30094678
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Biological sciences
Microbiology
Engineering
Environmental engineering
Nanotechnology
Calcium magnesium aluminate
Tri-metal aluminates
Electrochemical studies
Sensing
Photocatalysis
Acid orange-88
Anti-microbial studies
dc.title.none.fl_str_mv Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">Aloe vera (Aloe barbadensis miller) leaf extract was used in green fuel-assisted microwave synthesis to prepare Calcium Magnesium Aluminate (CMA). The synthesized CMA was characterized by X-ray diffraction (XRD), Fourier transform-infrared (FT-IR), Scanning electron microscope (SEM), Energy dispersion spectrometer (EDAX), and Transmission Electron Microscopy (TEM) analyses. X-ray diffraction confirmed the formation of Ca<sub>2</sub>Mg<sub>2</sub>Al<sub>28</sub>O<sub>46</sub>. The UV–Vis diffuse reflectance (DRS) technique was employed to investigate its absorbance spectrum, and the band gap of CMA was found to be 4.9 eV. The CMA <u>nanoparticles</u> were used to design a sensing electrode for creatinine, enabling the determination of its concentration in human samples and heavy metals. Acid Orange-88 dye was degraded using CMA <u>nanoparticles</u> as a photocatalyst under UV irradiation. After dye degradation, treated water was used to grow Vigna radiata plants to test their suitability for seedling growth. This report demonstrates that CMA photocatalysts are alternatives to semiconductor photocatalysts for the degradation of Acid Orange-88 dye under UV illumination. <i>Escherichia coli</i> (E. coli), Staphylococcus species, and <i>Pseudomonas</i> species were used as model organisms to assess the antibacterial activity of CMA NPs through a green route.</p><h2>Other Information</h2><p dir="ltr">Published in: Inorganic Chemistry Communications<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.inoche.2024.113185" target="_blank">https://dx.doi.org/10.1016/j.inoche.2024.113185</a></p>
eu_rights_str_mv openAccess
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identifier_str_mv 10.1016/j.inoche.2024.113185
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/30094678
publishDate 2024
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spelling Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applicationsH.V. Harini (22224871)H.P. Nagaswarupa (22224874)Ramachandra Naik (22224877)L. Guddi Likmaram (22224880)S.K. Sukrutha (22224883)S.N. Pramod (22224886)Ramyakrishna Pothu (17792591)Mika Sillanpää (765189)Rajender Boddula (4636810)Ahmed Bahgat Radwan (17380297)Noora Al-Qahtani (15314043)Biological sciencesMicrobiologyEngineeringEnvironmental engineeringNanotechnologyCalcium magnesium aluminateTri-metal aluminatesElectrochemical studiesSensingPhotocatalysisAcid orange-88Anti-microbial studies<p dir="ltr">Aloe vera (Aloe barbadensis miller) leaf extract was used in green fuel-assisted microwave synthesis to prepare Calcium Magnesium Aluminate (CMA). The synthesized CMA was characterized by X-ray diffraction (XRD), Fourier transform-infrared (FT-IR), Scanning electron microscope (SEM), Energy dispersion spectrometer (EDAX), and Transmission Electron Microscopy (TEM) analyses. X-ray diffraction confirmed the formation of Ca<sub>2</sub>Mg<sub>2</sub>Al<sub>28</sub>O<sub>46</sub>. The UV–Vis diffuse reflectance (DRS) technique was employed to investigate its absorbance spectrum, and the band gap of CMA was found to be 4.9 eV. The CMA <u>nanoparticles</u> were used to design a sensing electrode for creatinine, enabling the determination of its concentration in human samples and heavy metals. Acid Orange-88 dye was degraded using CMA <u>nanoparticles</u> as a photocatalyst under UV irradiation. After dye degradation, treated water was used to grow Vigna radiata plants to test their suitability for seedling growth. This report demonstrates that CMA photocatalysts are alternatives to semiconductor photocatalysts for the degradation of Acid Orange-88 dye under UV illumination. <i>Escherichia coli</i> (E. coli), Staphylococcus species, and <i>Pseudomonas</i> species were used as model organisms to assess the antibacterial activity of CMA NPs through a green route.</p><h2>Other Information</h2><p dir="ltr">Published in: Inorganic Chemistry Communications<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.inoche.2024.113185" target="_blank">https://dx.doi.org/10.1016/j.inoche.2024.113185</a></p>2024-09-27T15:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.inoche.2024.113185https://figshare.com/articles/journal_contribution/Bioinspired_synthesis_of_calcium_magnesium_aluminate_nanoparticles_using_aloe_vera_extract_A_promising_material_for_electrochemical_sensors_antibacterial_and_environmental_remediation_applications/30094678CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/300946782024-09-27T15:00:00Z
spellingShingle Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications
H.V. Harini (22224871)
Biological sciences
Microbiology
Engineering
Environmental engineering
Nanotechnology
Calcium magnesium aluminate
Tri-metal aluminates
Electrochemical studies
Sensing
Photocatalysis
Acid orange-88
Anti-microbial studies
status_str publishedVersion
title Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications
title_full Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications
title_fullStr Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications
title_full_unstemmed Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications
title_short Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications
title_sort Bioinspired synthesis of calcium magnesium aluminate nanoparticles using aloe vera extract: A promising material for electrochemical sensors, antibacterial and environmental remediation applications
topic Biological sciences
Microbiology
Engineering
Environmental engineering
Nanotechnology
Calcium magnesium aluminate
Tri-metal aluminates
Electrochemical studies
Sensing
Photocatalysis
Acid orange-88
Anti-microbial studies