Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels

<p dir="ltr">This paper presents a rheological study describing the effects of shear on the flow curves of colloidal gels prepared with different concentrations of fumed silica (4%, 5%, 6%, and 7%) and a hydrophobic solvent (Hydrocarbon fuel, JP-8). Viscosity measurements as a functi...

وصف كامل

محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Paulo Santos (488565) (author)
مؤلفون آخرون: Marcelo Carignano (1390921) (author), Osvaldo Campanella (1768339) (author)
منشور في: 2017
الموضوعات:
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author Paulo Santos (488565)
author2 Marcelo Carignano (1390921)
Osvaldo Campanella (1768339)
author2_role author
author
author_facet Paulo Santos (488565)
Marcelo Carignano (1390921)
Osvaldo Campanella (1768339)
author_role author
dc.creator.none.fl_str_mv Paulo Santos (488565)
Marcelo Carignano (1390921)
Osvaldo Campanella (1768339)
dc.date.none.fl_str_mv 2017-11-20T03:00:00Z
dc.identifier.none.fl_str_mv 10.3390/gels3040045
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Effect_of_Shear_History_on_Rheology_of_Time-Dependent_Colloidal_Silica_Gels/27082714
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Engineering
Chemical engineering
Fluid mechanics and thermal engineering
gel
silica
rheology
thixotropy
microstructure
viscosity
JP-8
fuel
dc.title.none.fl_str_mv Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">This paper presents a rheological study describing the effects of shear on the flow curves of colloidal gels prepared with different concentrations of fumed silica (4%, 5%, 6%, and 7%) and a hydrophobic solvent (Hydrocarbon fuel, JP-8). Viscosity measurements as a function of time were carried out at different shear rates (10, 50, 100, 500, and 1000 s<sup>−1</sup>), and based on this data, a new structural kinetics model was used to describe the system. Previous work has based the analysis of time dependent fluids on the viscosity of the intact material, i.e., before it is sheared, which is a condition very difficult to achieve when weak gels are tested. The simple action of loading the gel in the rheometer affects its structure and rheology, and the reproducibility of the measurements is thus seriously compromised. Changes in viscosity and viscoelastic properties of the sheared material are indicative of microstructural changes in the gel that need to be accounted for. Therefore, a more realistic method is presented in this work. In addition, microscopical images (Cryo-SEM) were obtained to show how the structure of the gel is affected upon application of shear.</p><h2>Other Information</h2><p dir="ltr">Published in: Gels<br>License: <a href="https://creativecommons.org/licenses/by/4.0/" target="_blank">https://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.3390/gels3040045" target="_blank">https://dx.doi.org/10.3390/gels3040045</a></p>
eu_rights_str_mv openAccess
id Manara2_1d4722e30b693f164587a6ae51b99daf
identifier_str_mv 10.3390/gels3040045
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/27082714
publishDate 2017
repository.mail.fl_str_mv
repository.name.fl_str_mv
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rights_invalid_str_mv CC BY 4.0
spelling Effect of Shear History on Rheology of Time-Dependent Colloidal Silica GelsPaulo Santos (488565)Marcelo Carignano (1390921)Osvaldo Campanella (1768339)EngineeringChemical engineeringFluid mechanics and thermal engineeringgelsilicarheologythixotropymicrostructureviscosityJP-8fuel<p dir="ltr">This paper presents a rheological study describing the effects of shear on the flow curves of colloidal gels prepared with different concentrations of fumed silica (4%, 5%, 6%, and 7%) and a hydrophobic solvent (Hydrocarbon fuel, JP-8). Viscosity measurements as a function of time were carried out at different shear rates (10, 50, 100, 500, and 1000 s<sup>−1</sup>), and based on this data, a new structural kinetics model was used to describe the system. Previous work has based the analysis of time dependent fluids on the viscosity of the intact material, i.e., before it is sheared, which is a condition very difficult to achieve when weak gels are tested. The simple action of loading the gel in the rheometer affects its structure and rheology, and the reproducibility of the measurements is thus seriously compromised. Changes in viscosity and viscoelastic properties of the sheared material are indicative of microstructural changes in the gel that need to be accounted for. Therefore, a more realistic method is presented in this work. In addition, microscopical images (Cryo-SEM) were obtained to show how the structure of the gel is affected upon application of shear.</p><h2>Other Information</h2><p dir="ltr">Published in: Gels<br>License: <a href="https://creativecommons.org/licenses/by/4.0/" target="_blank">https://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.3390/gels3040045" target="_blank">https://dx.doi.org/10.3390/gels3040045</a></p>2017-11-20T03:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.3390/gels3040045https://figshare.com/articles/journal_contribution/Effect_of_Shear_History_on_Rheology_of_Time-Dependent_Colloidal_Silica_Gels/27082714CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/270827142017-11-20T03:00:00Z
spellingShingle Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels
Paulo Santos (488565)
Engineering
Chemical engineering
Fluid mechanics and thermal engineering
gel
silica
rheology
thixotropy
microstructure
viscosity
JP-8
fuel
status_str publishedVersion
title Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels
title_full Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels
title_fullStr Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels
title_full_unstemmed Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels
title_short Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels
title_sort Effect of Shear History on Rheology of Time-Dependent Colloidal Silica Gels
topic Engineering
Chemical engineering
Fluid mechanics and thermal engineering
gel
silica
rheology
thixotropy
microstructure
viscosity
JP-8
fuel