In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals

<p dir="ltr">An efficient multi-functional electrolyzer with a Ni- and Fe-layered double hydroxide (NiFe-LDH) anode and a binary NiMo cathode is designed for overall water splitting coupled with the desalination of saline water and production of value-added chemicals. The NiFe-LDH an...

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محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Byeong-ju Kim (7320773) (author)
مؤلفون آخرون: Ho Kyong Shon (2092561) (author), Dong Suk Han (1748989) (author), Hyunwoong Park (1521754) (author)
منشور في: 2023
الموضوعات:
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author Byeong-ju Kim (7320773)
author2 Ho Kyong Shon (2092561)
Dong Suk Han (1748989)
Hyunwoong Park (1521754)
author2_role author
author
author
author_facet Byeong-ju Kim (7320773)
Ho Kyong Shon (2092561)
Dong Suk Han (1748989)
Hyunwoong Park (1521754)
author_role author
dc.creator.none.fl_str_mv Byeong-ju Kim (7320773)
Ho Kyong Shon (2092561)
Dong Suk Han (1748989)
Hyunwoong Park (1521754)
dc.date.none.fl_str_mv 2023-04-01T00:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.desal.2023.116431
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/In-situ_desalination-coupled_electrolysis_with_concurrent_one-step-synthesis_of_value-added_chemicals/25036427
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Physical chemistry
Engineering
Chemical engineering
Materials engineering
Desalination
Bipolar membrane
Electrocatalysis
Seawater electrolysis
Acid and base
dc.title.none.fl_str_mv In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">An efficient multi-functional electrolyzer with a Ni- and Fe-layered double hydroxide (NiFe-LDH) anode and a binary NiMo cathode is designed for overall water splitting coupled with the desalination of saline water and production of value-added chemicals. The NiFe-LDH and NiMo pairs separated by a bipolar membrane (BPM) show overpotentials as low as those of noble metal catalysts for oxygen and hydrogen evolution reactions in 1 M KOH and 1 M H<sub>2</sub>SO<sub>4</sub> solutions, respectively. Arraying anion and cation-exchange membranes (AEMs and CEMs, respectively) with BPMs (NiFe-LDH/BPM/[AEM/CEM] n /BPM/NiMo; n = 1 or 5) further enables the desalination of brackish water and seawater at specific energy consumption of 1.8 kWh m<sup>−3</sup>, with concurrent production of HCl and NaOH. The Faradaic efficiencies of the device for O<sub>2</sub> and H<sub>2</sub> production are >95 % at J = 100 mA cm<sup>−2</sup> over 20 h, while the initial pH values of the anolyte and catholyte remain unchanged. Detailed surface characterization of the electrocatalysts is performed, and various electrolyzer configurations are compared in terms of desalination efficiency.</p><h2>Other Information</h2><p dir="ltr">Published in: Desalination<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.desal.2023.116431" target="_blank">https://dx.doi.org/10.1016/j.desal.2023.116431</a></p>
eu_rights_str_mv openAccess
id Manara2_2a439fec75b9b65a9a6f7ef0f8ac456f
identifier_str_mv 10.1016/j.desal.2023.116431
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/25036427
publishDate 2023
repository.mail.fl_str_mv
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rights_invalid_str_mv CC BY 4.0
spelling In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicalsByeong-ju Kim (7320773)Ho Kyong Shon (2092561)Dong Suk Han (1748989)Hyunwoong Park (1521754)Chemical sciencesPhysical chemistryEngineeringChemical engineeringMaterials engineeringDesalinationBipolar membraneElectrocatalysisSeawater electrolysisAcid and base<p dir="ltr">An efficient multi-functional electrolyzer with a Ni- and Fe-layered double hydroxide (NiFe-LDH) anode and a binary NiMo cathode is designed for overall water splitting coupled with the desalination of saline water and production of value-added chemicals. The NiFe-LDH and NiMo pairs separated by a bipolar membrane (BPM) show overpotentials as low as those of noble metal catalysts for oxygen and hydrogen evolution reactions in 1 M KOH and 1 M H<sub>2</sub>SO<sub>4</sub> solutions, respectively. Arraying anion and cation-exchange membranes (AEMs and CEMs, respectively) with BPMs (NiFe-LDH/BPM/[AEM/CEM] n /BPM/NiMo; n = 1 or 5) further enables the desalination of brackish water and seawater at specific energy consumption of 1.8 kWh m<sup>−3</sup>, with concurrent production of HCl and NaOH. The Faradaic efficiencies of the device for O<sub>2</sub> and H<sub>2</sub> production are >95 % at J = 100 mA cm<sup>−2</sup> over 20 h, while the initial pH values of the anolyte and catholyte remain unchanged. Detailed surface characterization of the electrocatalysts is performed, and various electrolyzer configurations are compared in terms of desalination efficiency.</p><h2>Other Information</h2><p dir="ltr">Published in: Desalination<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.desal.2023.116431" target="_blank">https://dx.doi.org/10.1016/j.desal.2023.116431</a></p>2023-04-01T00:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.desal.2023.116431https://figshare.com/articles/journal_contribution/In-situ_desalination-coupled_electrolysis_with_concurrent_one-step-synthesis_of_value-added_chemicals/25036427CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/250364272023-04-01T00:00:00Z
spellingShingle In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals
Byeong-ju Kim (7320773)
Chemical sciences
Physical chemistry
Engineering
Chemical engineering
Materials engineering
Desalination
Bipolar membrane
Electrocatalysis
Seawater electrolysis
Acid and base
status_str publishedVersion
title In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals
title_full In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals
title_fullStr In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals
title_full_unstemmed In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals
title_short In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals
title_sort In-situ desalination-coupled electrolysis with concurrent one-step-synthesis of value-added chemicals
topic Chemical sciences
Physical chemistry
Engineering
Chemical engineering
Materials engineering
Desalination
Bipolar membrane
Electrocatalysis
Seawater electrolysis
Acid and base