Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions

<p dir="ltr">In solid-liquid separation processes, coagulation/flocculation is one of the most popular techniques in treating wastewater, as it is efficient, simple, and economical. Consequently, the formation of a new environment friendly destabilizing agent needed for the developme...

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محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Dana I.M. Al-Risheq (16932606) (author)
مؤلفون آخرون: M.S. Nasser (17075293) (author), Hazim Qiblawey (16030546) (author), Ibnelwaleed A. Hussein (5535953) (author), Abdelbaki Benamor (2868371) (author)
منشور في: 2021
الموضوعات:
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author Dana I.M. Al-Risheq (16932606)
author2 M.S. Nasser (17075293)
Hazim Qiblawey (16030546)
Ibnelwaleed A. Hussein (5535953)
Abdelbaki Benamor (2868371)
author2_role author
author
author
author
author_facet Dana I.M. Al-Risheq (16932606)
M.S. Nasser (17075293)
Hazim Qiblawey (16030546)
Ibnelwaleed A. Hussein (5535953)
Abdelbaki Benamor (2868371)
author_role author
dc.creator.none.fl_str_mv Dana I.M. Al-Risheq (16932606)
M.S. Nasser (17075293)
Hazim Qiblawey (16030546)
Ibnelwaleed A. Hussein (5535953)
Abdelbaki Benamor (2868371)
dc.date.none.fl_str_mv 2021-01-15T00:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.seppur.2020.117737
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Choline_chloride_based_natural_deep_eutectic_solvent_for_destabilization_and_separation_of_stable_colloidal_dispersions/24225694
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Analytical chemistry
Engineering
Chemical engineering
Bentonite
Coagulation
NADES
Turbidity
Zeta potential
Floc size
Settling behaviour
dc.title.none.fl_str_mv Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">In solid-liquid separation processes, coagulation/flocculation is one of the most popular techniques in treating wastewater, as it is efficient, simple, and economical. Consequently, the formation of a new environment friendly destabilizing agent needed for the development of this processes. Hence, the aim of this paper is to introduce a new green and cheap choline chloride (ChCl) based natural deep eutectic solvent (NADES) as a coagulant for clay-based dispersions which are known to be a highly stable colloidal systems. For the NADES preparation, lactic acid (LA) and ChCl were used as the hydrogen bond donor and acceptor, respectively with a 1:1 ratio. Furthermore, the individual components of the NADES; ChCl and LA were also separately tested as coagulants as well as a binary mixture of both. Zeta potential, turbidity, floc size distribution, settling behavior, and viscosity measurements were conducted to study the potential of NADES in destabilizing and separating of high-stable bentonite dispersions and determine the strength of the resultant flocs. Initially, at pH 10, bentonite suspension had a high turbidity of 347 NTU and zeta potential of − 45 mV. At optimum concentration the reduction in turbidity and zeta potential were as follows: 5.32 NTU with − 30.6 mV, and 4.3 NTU with − 22 mV was achieved using ChCl alone and mixture of ChCl and LA (ChCl-Cl), respectively. NADES showed the most efficient performance with almost 100% turbidity removal and a significant reduction in the zeta potential of − 18 mV. For the three tested coagulants (ChCl, ChCl-LA, and NADES), produced flocs ranged in size from 5 μm to 36 μm depending on the coagulant type and dosage were achieved. NADES produced the largest flocs followed by ChClLA and ChCl. The obtained results were also confirmed through settling rate and sediment volume in addition to the viscosity measurements of the resultant flocs</p><h2>Other Information</h2><p dir="ltr">Published in: Separation and Purification Technology<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.seppur.2020.117737" target="_blank">https://dx.doi.org/10.1016/j.seppur.2020.117737</a></p>
eu_rights_str_mv openAccess
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identifier_str_mv 10.1016/j.seppur.2020.117737
network_acronym_str Manara2
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oai_identifier_str oai:figshare.com:article/24225694
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spelling Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersionsDana I.M. Al-Risheq (16932606)M.S. Nasser (17075293)Hazim Qiblawey (16030546)Ibnelwaleed A. Hussein (5535953)Abdelbaki Benamor (2868371)Chemical sciencesAnalytical chemistryEngineeringChemical engineeringBentoniteCoagulationNADESTurbidityZeta potentialFloc sizeSettling behaviour<p dir="ltr">In solid-liquid separation processes, coagulation/flocculation is one of the most popular techniques in treating wastewater, as it is efficient, simple, and economical. Consequently, the formation of a new environment friendly destabilizing agent needed for the development of this processes. Hence, the aim of this paper is to introduce a new green and cheap choline chloride (ChCl) based natural deep eutectic solvent (NADES) as a coagulant for clay-based dispersions which are known to be a highly stable colloidal systems. For the NADES preparation, lactic acid (LA) and ChCl were used as the hydrogen bond donor and acceptor, respectively with a 1:1 ratio. Furthermore, the individual components of the NADES; ChCl and LA were also separately tested as coagulants as well as a binary mixture of both. Zeta potential, turbidity, floc size distribution, settling behavior, and viscosity measurements were conducted to study the potential of NADES in destabilizing and separating of high-stable bentonite dispersions and determine the strength of the resultant flocs. Initially, at pH 10, bentonite suspension had a high turbidity of 347 NTU and zeta potential of − 45 mV. At optimum concentration the reduction in turbidity and zeta potential were as follows: 5.32 NTU with − 30.6 mV, and 4.3 NTU with − 22 mV was achieved using ChCl alone and mixture of ChCl and LA (ChCl-Cl), respectively. NADES showed the most efficient performance with almost 100% turbidity removal and a significant reduction in the zeta potential of − 18 mV. For the three tested coagulants (ChCl, ChCl-LA, and NADES), produced flocs ranged in size from 5 μm to 36 μm depending on the coagulant type and dosage were achieved. NADES produced the largest flocs followed by ChClLA and ChCl. The obtained results were also confirmed through settling rate and sediment volume in addition to the viscosity measurements of the resultant flocs</p><h2>Other Information</h2><p dir="ltr">Published in: Separation and Purification Technology<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.seppur.2020.117737" target="_blank">https://dx.doi.org/10.1016/j.seppur.2020.117737</a></p>2021-01-15T00:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.seppur.2020.117737https://figshare.com/articles/journal_contribution/Choline_chloride_based_natural_deep_eutectic_solvent_for_destabilization_and_separation_of_stable_colloidal_dispersions/24225694CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/242256942021-01-15T00:00:00Z
spellingShingle Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions
Dana I.M. Al-Risheq (16932606)
Chemical sciences
Analytical chemistry
Engineering
Chemical engineering
Bentonite
Coagulation
NADES
Turbidity
Zeta potential
Floc size
Settling behaviour
status_str publishedVersion
title Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions
title_full Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions
title_fullStr Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions
title_full_unstemmed Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions
title_short Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions
title_sort Choline chloride based natural deep eutectic solvent for destabilization and separation of stable colloidal dispersions
topic Chemical sciences
Analytical chemistry
Engineering
Chemical engineering
Bentonite
Coagulation
NADES
Turbidity
Zeta potential
Floc size
Settling behaviour