An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte

<p><br></p><p dir="ltr">A plastic crystal, solid electrolyte was prepared by mixing tetrabutylammonium hexafluorophosphate salt, (C<sub>4</sub>H<sub>9</sub>)<sub>4</sub>-NPF<sub>6</sub>, (10 molar %) with succinonitril...

وصف كامل

محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Ali Abouimrane (1954003) (author)
مؤلفون آخرون: Ilias Belharouak (1674784) (author), Yaser A. Abu-Lebdeh (19694467) (author)
منشور في: 2015
الموضوعات:
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author Ali Abouimrane (1954003)
author2 Ilias Belharouak (1674784)
Yaser A. Abu-Lebdeh (19694467)
author2_role author
author
author_facet Ali Abouimrane (1954003)
Ilias Belharouak (1674784)
Yaser A. Abu-Lebdeh (19694467)
author_role author
dc.creator.none.fl_str_mv Ali Abouimrane (1954003)
Ilias Belharouak (1674784)
Yaser A. Abu-Lebdeh (19694467)
dc.date.none.fl_str_mv 2015-08-18T06:00:00Z
dc.identifier.none.fl_str_mv 10.3389/fenrg.2015.00034
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/An_All-Solid-State_Electrochemical_Double-Layer_Capacitor_Based_on_a_Plastic_Crystal_Electrolyte/27051607
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Physical chemistry
Engineering
Materials engineering
plastic crystal
solid electrolyte
capacitor
uccinonitrile
EDLC
dc.title.none.fl_str_mv An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p><br></p><p dir="ltr">A plastic crystal, solid electrolyte was prepared by mixing tetrabutylammonium hexafluorophosphate salt, (C<sub>4</sub>H<sub>9</sub>)<sub>4</sub>-NPF<sub>6</sub>, (10 molar %) with succinonitrile, SCN, (N≡C−CH<sub>2</sub>−CH<sub>2</sub>−C≡N), [SCN-10%TBA-PF<sub>6</sub>]. The resultant waxy material shows a plastic crystalline phase that extends from −36°C up to its melting at 23°C. It shows a high ionic conductivity reaching 4×10<sup>-5</sup> S/cm in the plastic crystal phase (15°C) and ~ 3×10<sup>-3</sup> S/cm in the molten state (25°C). These properties along with the high electrochemical stability rendered the use of this material as an electrolyte in an electrochemical double-layer capacitor (EDLC). The EDLC was assembled, and its performance was tested by cyclic voltammetry, AC impedance spectroscopy, and galvanostatic charge–discharge methods. Specific capacitance values in the range of 4–7 F/g (of electrode active material) were obtained in the plastic crystal phase at 15°C, that although compare well with those reported for some polymer electrolytes, can be still enhanced with further development of the device and its components, and only demonstrate their great potential use for capacitors as a new application.</p><h2>Other Information</h2><p dir="ltr">Published in: Frontiers in Energy Research<br>License: <a href="https://creativecommons.org/licenses/by/4.0/" rel="noreferrer" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.3389/fenrg.2015.00034" target="_blank">https://dx.doi.org/10.3389/fenrg.2015.00034</a></p>
eu_rights_str_mv openAccess
id Manara2_4a0a6845df23e01b6808f9f7980484cc
identifier_str_mv 10.3389/fenrg.2015.00034
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/27051607
publishDate 2015
repository.mail.fl_str_mv
repository.name.fl_str_mv
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rights_invalid_str_mv CC BY 4.0
spelling An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal ElectrolyteAli Abouimrane (1954003)Ilias Belharouak (1674784)Yaser A. Abu-Lebdeh (19694467)Chemical sciencesPhysical chemistryEngineeringMaterials engineeringplastic crystalsolid electrolytecapacitoruccinonitrileEDLC<p><br></p><p dir="ltr">A plastic crystal, solid electrolyte was prepared by mixing tetrabutylammonium hexafluorophosphate salt, (C<sub>4</sub>H<sub>9</sub>)<sub>4</sub>-NPF<sub>6</sub>, (10 molar %) with succinonitrile, SCN, (N≡C−CH<sub>2</sub>−CH<sub>2</sub>−C≡N), [SCN-10%TBA-PF<sub>6</sub>]. The resultant waxy material shows a plastic crystalline phase that extends from −36°C up to its melting at 23°C. It shows a high ionic conductivity reaching 4×10<sup>-5</sup> S/cm in the plastic crystal phase (15°C) and ~ 3×10<sup>-3</sup> S/cm in the molten state (25°C). These properties along with the high electrochemical stability rendered the use of this material as an electrolyte in an electrochemical double-layer capacitor (EDLC). The EDLC was assembled, and its performance was tested by cyclic voltammetry, AC impedance spectroscopy, and galvanostatic charge–discharge methods. Specific capacitance values in the range of 4–7 F/g (of electrode active material) were obtained in the plastic crystal phase at 15°C, that although compare well with those reported for some polymer electrolytes, can be still enhanced with further development of the device and its components, and only demonstrate their great potential use for capacitors as a new application.</p><h2>Other Information</h2><p dir="ltr">Published in: Frontiers in Energy Research<br>License: <a href="https://creativecommons.org/licenses/by/4.0/" rel="noreferrer" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.3389/fenrg.2015.00034" target="_blank">https://dx.doi.org/10.3389/fenrg.2015.00034</a></p>2015-08-18T06:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.3389/fenrg.2015.00034https://figshare.com/articles/journal_contribution/An_All-Solid-State_Electrochemical_Double-Layer_Capacitor_Based_on_a_Plastic_Crystal_Electrolyte/27051607CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/270516072015-08-18T06:00:00Z
spellingShingle An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte
Ali Abouimrane (1954003)
Chemical sciences
Physical chemistry
Engineering
Materials engineering
plastic crystal
solid electrolyte
capacitor
uccinonitrile
EDLC
status_str publishedVersion
title An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte
title_full An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte
title_fullStr An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte
title_full_unstemmed An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte
title_short An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte
title_sort An All-Solid-State Electrochemical Double-Layer Capacitor Based on a Plastic Crystal Electrolyte
topic Chemical sciences
Physical chemistry
Engineering
Materials engineering
plastic crystal
solid electrolyte
capacitor
uccinonitrile
EDLC