Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels

<p dir="ltr">Synthesis, characterization, and application of Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials (where, Ln = La, Pr, Nd, Sm, Gd, Tb, Dy, Er) for the thermochemical conversi...

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محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Gorakshnath Takalkar (14151135) (author)
مؤلفون آخرون: Rahul R. Bhosale (6467102) (author), Fares AlMomani (14097725) (author), Suliman Rashid (14151138) (author)
منشور في: 2020
الموضوعات:
الوسوم: إضافة وسم
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_version_ 1864513552079912960
author Gorakshnath Takalkar (14151135)
author2 Rahul R. Bhosale (6467102)
Fares AlMomani (14097725)
Suliman Rashid (14151138)
author2_role author
author
author
author_facet Gorakshnath Takalkar (14151135)
Rahul R. Bhosale (6467102)
Fares AlMomani (14097725)
Suliman Rashid (14151138)
author_role author
dc.creator.none.fl_str_mv Gorakshnath Takalkar (14151135)
Rahul R. Bhosale (6467102)
Fares AlMomani (14097725)
Suliman Rashid (14151138)
dc.date.none.fl_str_mv 2020-03-27T21:00:00Z
dc.identifier.none.fl_str_mv 10.1007/s10853-020-04567-w
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Co-precipitation_synthesized_nanostructured_Ce0_9Ln0_05Ag0_05O2_materials_for_solar_thermochemical_conversion_of_CO2_into_fuels/21597303
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Engineering
Materials engineering
Mechanical engineering
Synthesis
Co-precipitation method
Nanostructured particles
Redox reactivity
Oxygen release
CO2 splitting
Catalytic performance
dc.title.none.fl_str_mv Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">Synthesis, characterization, and application of Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials (where, Ln = La, Pr, Nd, Sm, Gd, Tb, Dy, Er) for the thermochemical conversion of CO2 reported in this paper. The Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials were synthesized by using an ammonium hydroxide-driven co-precipitation method. The derived Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials were characterized via powder X-ray diffraction, scanning electron microscope, and electron diffraction spectroscopy. The characterization results indicate the formation of spherically shaped Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> nanostructured particles. As-prepared Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials were further tested toward multiple CO<sub>2</sub> splitting cycles by utilizing a thermogravimetric analyzer. The results obtained indicate that all the Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials produced higher quantities of O<sub>2</sub> and CO than the previously studied pure CeO<sub>2 </sub>and lanthanide-doped ceria materials. Overall, the Ce<sub>0.911</sub>La<sub>0</sub>.<sub>053</sub>Ag<sub>0.047O1.925</sub> showed the maximum redox reactivity in terms of O<sub>2</sub> release (72.2 μmol/g cycle) and CO production (136.6 μmol/g cycle).</p><h2>Other Information</h2><p dir="ltr">Published in: Journal of Materials Science<br>License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="http://dx.doi.org/10.1007/s10853-020-04567-w" target="_blank">http://dx.doi.org/10.1007/s10853-020-04567-w</a></p>
eu_rights_str_mv openAccess
id Manara2_5c0d0e542ca52563576be654d03b20dc
identifier_str_mv 10.1007/s10853-020-04567-w
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/21597303
publishDate 2020
repository.mail.fl_str_mv
repository.name.fl_str_mv
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rights_invalid_str_mv CC BY 4.0
spelling Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuelsGorakshnath Takalkar (14151135)Rahul R. Bhosale (6467102)Fares AlMomani (14097725)Suliman Rashid (14151138)EngineeringMaterials engineeringMechanical engineeringSynthesisCo-precipitation methodNanostructured particlesRedox reactivityOxygen releaseCO2 splittingCatalytic performance<p dir="ltr">Synthesis, characterization, and application of Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials (where, Ln = La, Pr, Nd, Sm, Gd, Tb, Dy, Er) for the thermochemical conversion of CO2 reported in this paper. The Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials were synthesized by using an ammonium hydroxide-driven co-precipitation method. The derived Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials were characterized via powder X-ray diffraction, scanning electron microscope, and electron diffraction spectroscopy. The characterization results indicate the formation of spherically shaped Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> nanostructured particles. As-prepared Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials were further tested toward multiple CO<sub>2</sub> splitting cycles by utilizing a thermogravimetric analyzer. The results obtained indicate that all the Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials produced higher quantities of O<sub>2</sub> and CO than the previously studied pure CeO<sub>2 </sub>and lanthanide-doped ceria materials. Overall, the Ce<sub>0.911</sub>La<sub>0</sub>.<sub>053</sub>Ag<sub>0.047O1.925</sub> showed the maximum redox reactivity in terms of O<sub>2</sub> release (72.2 μmol/g cycle) and CO production (136.6 μmol/g cycle).</p><h2>Other Information</h2><p dir="ltr">Published in: Journal of Materials Science<br>License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="http://dx.doi.org/10.1007/s10853-020-04567-w" target="_blank">http://dx.doi.org/10.1007/s10853-020-04567-w</a></p>2020-03-27T21:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1007/s10853-020-04567-whttps://figshare.com/articles/journal_contribution/Co-precipitation_synthesized_nanostructured_Ce0_9Ln0_05Ag0_05O2_materials_for_solar_thermochemical_conversion_of_CO2_into_fuels/21597303CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/215973032020-03-27T21:00:00Z
spellingShingle Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels
Gorakshnath Takalkar (14151135)
Engineering
Materials engineering
Mechanical engineering
Synthesis
Co-precipitation method
Nanostructured particles
Redox reactivity
Oxygen release
CO2 splitting
Catalytic performance
status_str publishedVersion
title Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels
title_full Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels
title_fullStr Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels
title_full_unstemmed Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels
title_short Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels
title_sort Co-precipitation synthesized nanostructured Ce<sub>0.9</sub>Ln0.<sub>05</sub>Ag0.<sub>05</sub>O<sub>2</sub><sub>−δ</sub> materials for solar thermochemical conversion of CO<sub>2</sub> into fuels
topic Engineering
Materials engineering
Mechanical engineering
Synthesis
Co-precipitation method
Nanostructured particles
Redox reactivity
Oxygen release
CO2 splitting
Catalytic performance