Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries

<p dir="ltr">Transition metal layered oxide materials with a general formula Na<sub>x</sub>MO<sub>2</sub> (M = Ni, Mn, Co, Fe) are widely researched with various possible electrode configurations. Herein, O3‐type NaNi<sub>(1−x)</sub>/<sub>2&l...

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Main Author: Buzaina Moossa (17337883) (author)
Other Authors: Jeffin James Abraham (14778238) (author), Ranasinghe Arachchige Harindi Gayara (17746929) (author), Abdul Moiz Ahmed (17746932) (author), Rana Faisal Shahzad (17746935) (author), Ramazan Kahraman (1766956) (author), Siham Al-Qaradawi (14151177) (author), Shahid Rasul (5146139) (author), Rana Abdul Shakoor (14151141) (author)
Published: 2023
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_version_ 1864513531006681088
author Buzaina Moossa (17337883)
author2 Jeffin James Abraham (14778238)
Ranasinghe Arachchige Harindi Gayara (17746929)
Abdul Moiz Ahmed (17746932)
Rana Faisal Shahzad (17746935)
Ramazan Kahraman (1766956)
Siham Al-Qaradawi (14151177)
Shahid Rasul (5146139)
Rana Abdul Shakoor (14151141)
author2_role author
author
author
author
author
author
author
author
author_facet Buzaina Moossa (17337883)
Jeffin James Abraham (14778238)
Ranasinghe Arachchige Harindi Gayara (17746929)
Abdul Moiz Ahmed (17746932)
Rana Faisal Shahzad (17746935)
Ramazan Kahraman (1766956)
Siham Al-Qaradawi (14151177)
Shahid Rasul (5146139)
Rana Abdul Shakoor (14151141)
author_role author
dc.creator.none.fl_str_mv Buzaina Moossa (17337883)
Jeffin James Abraham (14778238)
Ranasinghe Arachchige Harindi Gayara (17746929)
Abdul Moiz Ahmed (17746932)
Rana Faisal Shahzad (17746935)
Ramazan Kahraman (1766956)
Siham Al-Qaradawi (14151177)
Shahid Rasul (5146139)
Rana Abdul Shakoor (14151141)
dc.date.none.fl_str_mv 2023-08-09T03:00:00Z
dc.identifier.none.fl_str_mv 10.1002/ente.202300437
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Molybdenum_Incorporated_O3_type_Sodium_Layered_Oxide_Cathodes_for_High_Performance_Sodium_Ion_Batteries/24954741
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Physical chemistry
Engineering
Materials engineering
O3-type
Sodium Layered
Oxide Cathodes
Sodium-Ion Batteries
dc.title.none.fl_str_mv Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">Transition metal layered oxide materials with a general formula Na<sub>x</sub>MO<sub>2</sub> (M = Ni, Mn, Co, Fe) are widely researched with various possible electrode configurations. Herein, O3‐type NaNi<sub>(1−x)</sub>/<sub>2</sub>Mn<sub>(1−x)</sub>/<sub>2</sub>Mo<sub>x</sub>O<sub>2</sub> (x = 0, 0.05,0.1) layered oxide cathode materials are synthesized by solid‐state reaction method, and its structural, thermal, and electrochemical performance in sodium ion battery is investigated. The structural analysis reveals that a single phase highly crystalline O3‐type cathode material with an irregular particle shape is formed. The introduction of molybdenum improves the thermal stability of cathode materials, which can be attributed to the improved TMO<sub>2</sub> layers that provide stability to the material. The addition of Mo to Na‐layered oxide cathode materials enhances electrochemical performance. The developed cathode materials, the NaNi<sub>0.475</sub>Mn<sub>0.475</sub>Mo<sub>0.05O2</sub>, exhibit excellent specific discharge capacity (≈154 mAh g<sup>−1</sup>) at C/20 rate, (an increase of ≈20% when compared to the NaNi<sub>0.5</sub>Mn<sub>0.5</sub>O<sub>2</sub>) which can be attributed to the increased capacitance effect by the addition of Mo. The electrochemical impedance spectroscopy study reveals that the diffusion of Na+ into/from the host structure is rapid during the first cycle and then gradually reduces with subsequent cycling due to the formation of the solid electrolyte interface layer, which hinders Na+ migration. This has a potential effect on the improved electrochemical performance of the material.</p><h2>Other Information</h2><p dir="ltr">Published in: Energy Technology<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1002/ente.202300437" target="_blank">https://dx.doi.org/10.1002/ente.202300437</a></p>
eu_rights_str_mv openAccess
id Manara2_6bdfe9ad44df9c0700e27ac2b8a45d3f
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network_acronym_str Manara2
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oai_identifier_str oai:figshare.com:article/24954741
publishDate 2023
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rights_invalid_str_mv CC BY 4.0
spelling Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion BatteriesBuzaina Moossa (17337883)Jeffin James Abraham (14778238)Ranasinghe Arachchige Harindi Gayara (17746929)Abdul Moiz Ahmed (17746932)Rana Faisal Shahzad (17746935)Ramazan Kahraman (1766956)Siham Al-Qaradawi (14151177)Shahid Rasul (5146139)Rana Abdul Shakoor (14151141)Chemical sciencesPhysical chemistryEngineeringMaterials engineeringO3-typeSodium LayeredOxide CathodesSodium-Ion Batteries<p dir="ltr">Transition metal layered oxide materials with a general formula Na<sub>x</sub>MO<sub>2</sub> (M = Ni, Mn, Co, Fe) are widely researched with various possible electrode configurations. Herein, O3‐type NaNi<sub>(1−x)</sub>/<sub>2</sub>Mn<sub>(1−x)</sub>/<sub>2</sub>Mo<sub>x</sub>O<sub>2</sub> (x = 0, 0.05,0.1) layered oxide cathode materials are synthesized by solid‐state reaction method, and its structural, thermal, and electrochemical performance in sodium ion battery is investigated. The structural analysis reveals that a single phase highly crystalline O3‐type cathode material with an irregular particle shape is formed. The introduction of molybdenum improves the thermal stability of cathode materials, which can be attributed to the improved TMO<sub>2</sub> layers that provide stability to the material. The addition of Mo to Na‐layered oxide cathode materials enhances electrochemical performance. The developed cathode materials, the NaNi<sub>0.475</sub>Mn<sub>0.475</sub>Mo<sub>0.05O2</sub>, exhibit excellent specific discharge capacity (≈154 mAh g<sup>−1</sup>) at C/20 rate, (an increase of ≈20% when compared to the NaNi<sub>0.5</sub>Mn<sub>0.5</sub>O<sub>2</sub>) which can be attributed to the increased capacitance effect by the addition of Mo. The electrochemical impedance spectroscopy study reveals that the diffusion of Na+ into/from the host structure is rapid during the first cycle and then gradually reduces with subsequent cycling due to the formation of the solid electrolyte interface layer, which hinders Na+ migration. This has a potential effect on the improved electrochemical performance of the material.</p><h2>Other Information</h2><p dir="ltr">Published in: Energy Technology<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1002/ente.202300437" target="_blank">https://dx.doi.org/10.1002/ente.202300437</a></p>2023-08-09T03:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1002/ente.202300437https://figshare.com/articles/journal_contribution/Molybdenum_Incorporated_O3_type_Sodium_Layered_Oxide_Cathodes_for_High_Performance_Sodium_Ion_Batteries/24954741CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/249547412023-08-09T03:00:00Z
spellingShingle Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries
Buzaina Moossa (17337883)
Chemical sciences
Physical chemistry
Engineering
Materials engineering
O3-type
Sodium Layered
Oxide Cathodes
Sodium-Ion Batteries
status_str publishedVersion
title Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries
title_full Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries
title_fullStr Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries
title_full_unstemmed Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries
title_short Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries
title_sort Molybdenum‐Incorporated O3‐type Sodium Layered Oxide Cathodes for High‐Performance Sodium‐Ion Batteries
topic Chemical sciences
Physical chemistry
Engineering
Materials engineering
O3-type
Sodium Layered
Oxide Cathodes
Sodium-Ion Batteries