Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study

<h3>Introduction</h3><p dir="ltr">Alzheimer’s Disease (AD) is complex and novel approaches are urgently needed to aid in diagnosis. Blood is frequently used as a source for biomarkers; however, its complexity prevents proper detection. The analytical power of metabolomics...

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التفاصيل البيبلوغرافية
المؤلف الرئيسي: Jonas Ellegaard Nielsen (21633062) (author)
مؤلفون آخرون: Trygve Andreassen (7373192) (author), Charlotte Held Gotfredsen (8350599) (author), Dorte Aalund Olsen (9191732) (author), Karsten Vestergaard (17016778) (author), Jonna Skov Madsen (5238674) (author), Søren Risom Kristensen (2792272) (author), Shona Pedersen (2792278) (author)
منشور في: 2024
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author Jonas Ellegaard Nielsen (21633062)
author2 Trygve Andreassen (7373192)
Charlotte Held Gotfredsen (8350599)
Dorte Aalund Olsen (9191732)
Karsten Vestergaard (17016778)
Jonna Skov Madsen (5238674)
Søren Risom Kristensen (2792272)
Shona Pedersen (2792278)
author2_role author
author
author
author
author
author
author
author_facet Jonas Ellegaard Nielsen (21633062)
Trygve Andreassen (7373192)
Charlotte Held Gotfredsen (8350599)
Dorte Aalund Olsen (9191732)
Karsten Vestergaard (17016778)
Jonna Skov Madsen (5238674)
Søren Risom Kristensen (2792272)
Shona Pedersen (2792278)
author_role author
dc.creator.none.fl_str_mv Jonas Ellegaard Nielsen (21633062)
Trygve Andreassen (7373192)
Charlotte Held Gotfredsen (8350599)
Dorte Aalund Olsen (9191732)
Karsten Vestergaard (17016778)
Jonna Skov Madsen (5238674)
Søren Risom Kristensen (2792272)
Shona Pedersen (2792278)
dc.date.none.fl_str_mv 2024-01-05T03:00:00Z
dc.identifier.none.fl_str_mv 10.1007/s11306-023-02078-8
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Serum_metabolic_signatures_for_Alzheimer_s_Disease_reveal_alterations_in_amino_acid_composition_a_validation_study/29445593
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Biomedical and clinical sciences
Medical biochemistry and metabolomics
Neurosciences
Alzheimer
Metabolites
Biomarker
Serum
Nuclear magnetic resonance
Single molecule array
dc.title.none.fl_str_mv Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <h3>Introduction</h3><p dir="ltr">Alzheimer’s Disease (AD) is complex and novel approaches are urgently needed to aid in diagnosis. Blood is frequently used as a source for biomarkers; however, its complexity prevents proper detection. The analytical power of metabolomics, coupled with statistical tools, can assist in reducing this complexity.</p><h3>Objectives</h3><p dir="ltr">Thus, we sought to validate a previously proposed panel of metabolic blood-based biomarkers for AD and expand our understanding of the pathological mechanisms involved in AD that are reflected in the blood.</p><h3>Methods</h3><p dir="ltr">In the validation cohort serum and plasma were collected from 25 AD patients and 25 healthy controls. Serum was analysed for metabolites using nuclear magnetic resonance (NMR) spectroscopy, while plasma was tested for markers of neuronal damage and AD hallmark proteins using single molecule array (SIMOA).</p><h3>Results</h3><p dir="ltr">The diagnostic performance of the metabolite biomarker panel was confirmed using sparse-partial least squares discriminant analysis (sPLS-DA) with an area under the curve (AUC) of 0.73 (95% confidence interval: 0.59–0.87). Pyruvic acid and valine were consistently reduced in the discovery and validation cohorts. Pathway analysis of significantly altered metabolites in the validation set revealed that they are involved in branched-chain amino acids (BCAAs) and energy metabolism (glycolysis and gluconeogenesis). Additionally, strong positive correlations were observed for valine and isoleucine between cerebrospinal fluid p-tau and t-tau.</p><h3>Conclusions</h3><p dir="ltr">Our proposed panel of metabolites was successfully validated using a combined approach of NMR and sPLS-DA. It was discovered that cognitive-impairment-related metabolites belong to BCAAs and are involved in energy metabolism.</p><h2>Other Information</h2><p dir="ltr">Published in: Metabolomics<br>License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1007/s11306-023-02078-8" target="_blank">https://dx.doi.org/10.1007/s11306-023-02078-8</a></p>
eu_rights_str_mv openAccess
id Manara2_85fb86c0ae41a13a714ea8d8c76174e3
identifier_str_mv 10.1007/s11306-023-02078-8
network_acronym_str Manara2
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oai_identifier_str oai:figshare.com:article/29445593
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spelling Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation studyJonas Ellegaard Nielsen (21633062)Trygve Andreassen (7373192)Charlotte Held Gotfredsen (8350599)Dorte Aalund Olsen (9191732)Karsten Vestergaard (17016778)Jonna Skov Madsen (5238674)Søren Risom Kristensen (2792272)Shona Pedersen (2792278)Biomedical and clinical sciencesMedical biochemistry and metabolomicsNeurosciencesAlzheimerMetabolitesBiomarkerSerumNuclear magnetic resonanceSingle molecule array<h3>Introduction</h3><p dir="ltr">Alzheimer’s Disease (AD) is complex and novel approaches are urgently needed to aid in diagnosis. Blood is frequently used as a source for biomarkers; however, its complexity prevents proper detection. The analytical power of metabolomics, coupled with statistical tools, can assist in reducing this complexity.</p><h3>Objectives</h3><p dir="ltr">Thus, we sought to validate a previously proposed panel of metabolic blood-based biomarkers for AD and expand our understanding of the pathological mechanisms involved in AD that are reflected in the blood.</p><h3>Methods</h3><p dir="ltr">In the validation cohort serum and plasma were collected from 25 AD patients and 25 healthy controls. Serum was analysed for metabolites using nuclear magnetic resonance (NMR) spectroscopy, while plasma was tested for markers of neuronal damage and AD hallmark proteins using single molecule array (SIMOA).</p><h3>Results</h3><p dir="ltr">The diagnostic performance of the metabolite biomarker panel was confirmed using sparse-partial least squares discriminant analysis (sPLS-DA) with an area under the curve (AUC) of 0.73 (95% confidence interval: 0.59–0.87). Pyruvic acid and valine were consistently reduced in the discovery and validation cohorts. Pathway analysis of significantly altered metabolites in the validation set revealed that they are involved in branched-chain amino acids (BCAAs) and energy metabolism (glycolysis and gluconeogenesis). Additionally, strong positive correlations were observed for valine and isoleucine between cerebrospinal fluid p-tau and t-tau.</p><h3>Conclusions</h3><p dir="ltr">Our proposed panel of metabolites was successfully validated using a combined approach of NMR and sPLS-DA. It was discovered that cognitive-impairment-related metabolites belong to BCAAs and are involved in energy metabolism.</p><h2>Other Information</h2><p dir="ltr">Published in: Metabolomics<br>License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1007/s11306-023-02078-8" target="_blank">https://dx.doi.org/10.1007/s11306-023-02078-8</a></p>2024-01-05T03:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1007/s11306-023-02078-8https://figshare.com/articles/journal_contribution/Serum_metabolic_signatures_for_Alzheimer_s_Disease_reveal_alterations_in_amino_acid_composition_a_validation_study/29445593CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/294455932024-01-05T03:00:00Z
spellingShingle Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study
Jonas Ellegaard Nielsen (21633062)
Biomedical and clinical sciences
Medical biochemistry and metabolomics
Neurosciences
Alzheimer
Metabolites
Biomarker
Serum
Nuclear magnetic resonance
Single molecule array
status_str publishedVersion
title Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study
title_full Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study
title_fullStr Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study
title_full_unstemmed Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study
title_short Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study
title_sort Serum metabolic signatures for Alzheimer’s Disease reveal alterations in amino acid composition: a validation study
topic Biomedical and clinical sciences
Medical biochemistry and metabolomics
Neurosciences
Alzheimer
Metabolites
Biomarker
Serum
Nuclear magnetic resonance
Single molecule array