Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer

<p>Triple negative breast cancer (TNBC) is considered the most aggressive type of breast malignancy. TNBC management approaches remain limited, with a high risk of relapse and metastasis. Chalcone compounds are established for their anticancer activity. A recently patented novel chalcone compo...

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Main Author: Azza Suliman (23124484) (author)
Other Authors: Arij Fouzat Hassan (21767516) (author), Sumayyah Saeed (23124487) (author), Ala-Eddin Al Moustafa (14153205) (author), Ashraf Khalil (4591618) (author), Abdelbary Elhissi (3397829) (author)
Published: 2025
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author Azza Suliman (23124484)
author2 Arij Fouzat Hassan (21767516)
Sumayyah Saeed (23124487)
Ala-Eddin Al Moustafa (14153205)
Ashraf Khalil (4591618)
Abdelbary Elhissi (3397829)
author2_role author
author
author
author
author
author_facet Azza Suliman (23124484)
Arij Fouzat Hassan (21767516)
Sumayyah Saeed (23124487)
Ala-Eddin Al Moustafa (14153205)
Ashraf Khalil (4591618)
Abdelbary Elhissi (3397829)
author_role author
dc.creator.none.fl_str_mv Azza Suliman (23124484)
Arij Fouzat Hassan (21767516)
Sumayyah Saeed (23124487)
Ala-Eddin Al Moustafa (14153205)
Ashraf Khalil (4591618)
Abdelbary Elhissi (3397829)
dc.date.none.fl_str_mv 2025-10-24T18:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.jddst.2025.107601
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Liposomal_delivery_of_DK14_chalcone_analogue_A_promising_therapeutic_strategy_against_triple-negative_breast_cancer/31239826
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Biomedical and clinical sciences
Oncology and carcinogenesis
Pharmacology and pharmaceutical sciences
Anticancer
Apoptosis
Breast cancer
Chalcone analogue
Metastasis
Liposome
dc.title.none.fl_str_mv Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p>Triple negative breast cancer (TNBC) is considered the most aggressive type of breast malignancy. TNBC management approaches remain limited, with a high risk of relapse and metastasis. Chalcone compounds are established for their anticancer activity. A recently patented novel chalcone compound (DK14) by our group has demonstrated a considerable activity against TNBC; however, its limited water-solubility is a challenge. In this study, we incorporated DK14 into a nano-liposomal formulation to enhance its solubility, safety and anticancer activity. The formulation was characterized in terms of particle size, zeta potential, drug entrapment, and release profile. Additionally, cytotoxicity, cell migration, colony formation and protein expression analysis were conducted. Furthermore, Angiogenesis study was performed using the chorioallantoic membrane (CAM) of the chicken embryo. DK14-liposomes demonstrated the ability to inhibit growth of TNBC cells and trigger apoptosis, accompanied by induction of BAX/BCL-2/Caspase-3 pathway. DK14-liposomes also exhibited an enhanced safety profile on non-tumorigenic mammary epithelial cells (MCF-10A) compared to free DK14 while suppressing cell migration and colony formation. Moreover, DK14-liposomes dysregulated PI3K/AKT/mTOR pathway, which is defective in TNBC; and significantly inhibited angiogenesis in ovo using a chiken embryo model. In conclusion, our results imply that DK14-liposomes have a substantial anticancer activity against TNBC with distinct anti-angiogenic properties.</p><h2>Other Information</h2> <p> Published in: Journal of Drug Delivery Science and Technology<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.jddst.2025.107601" target="_blank">https://dx.doi.org/10.1016/j.jddst.2025.107601</a></p>
eu_rights_str_mv openAccess
id Manara2_a4068034d31153bd0406e62428bd1f67
identifier_str_mv 10.1016/j.jddst.2025.107601
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/31239826
publishDate 2025
repository.mail.fl_str_mv
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rights_invalid_str_mv CC BY 4.0
spelling Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancerAzza Suliman (23124484)Arij Fouzat Hassan (21767516)Sumayyah Saeed (23124487)Ala-Eddin Al Moustafa (14153205)Ashraf Khalil (4591618)Abdelbary Elhissi (3397829)Biomedical and clinical sciencesOncology and carcinogenesisPharmacology and pharmaceutical sciencesAnticancerApoptosisBreast cancerChalcone analogueMetastasisLiposome<p>Triple negative breast cancer (TNBC) is considered the most aggressive type of breast malignancy. TNBC management approaches remain limited, with a high risk of relapse and metastasis. Chalcone compounds are established for their anticancer activity. A recently patented novel chalcone compound (DK14) by our group has demonstrated a considerable activity against TNBC; however, its limited water-solubility is a challenge. In this study, we incorporated DK14 into a nano-liposomal formulation to enhance its solubility, safety and anticancer activity. The formulation was characterized in terms of particle size, zeta potential, drug entrapment, and release profile. Additionally, cytotoxicity, cell migration, colony formation and protein expression analysis were conducted. Furthermore, Angiogenesis study was performed using the chorioallantoic membrane (CAM) of the chicken embryo. DK14-liposomes demonstrated the ability to inhibit growth of TNBC cells and trigger apoptosis, accompanied by induction of BAX/BCL-2/Caspase-3 pathway. DK14-liposomes also exhibited an enhanced safety profile on non-tumorigenic mammary epithelial cells (MCF-10A) compared to free DK14 while suppressing cell migration and colony formation. Moreover, DK14-liposomes dysregulated PI3K/AKT/mTOR pathway, which is defective in TNBC; and significantly inhibited angiogenesis in ovo using a chiken embryo model. In conclusion, our results imply that DK14-liposomes have a substantial anticancer activity against TNBC with distinct anti-angiogenic properties.</p><h2>Other Information</h2> <p> Published in: Journal of Drug Delivery Science and Technology<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.jddst.2025.107601" target="_blank">https://dx.doi.org/10.1016/j.jddst.2025.107601</a></p>2025-10-24T18:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.jddst.2025.107601https://figshare.com/articles/journal_contribution/Liposomal_delivery_of_DK14_chalcone_analogue_A_promising_therapeutic_strategy_against_triple-negative_breast_cancer/31239826CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/312398262025-10-24T18:00:00Z
spellingShingle Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer
Azza Suliman (23124484)
Biomedical and clinical sciences
Oncology and carcinogenesis
Pharmacology and pharmaceutical sciences
Anticancer
Apoptosis
Breast cancer
Chalcone analogue
Metastasis
Liposome
status_str publishedVersion
title Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer
title_full Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer
title_fullStr Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer
title_full_unstemmed Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer
title_short Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer
title_sort Liposomal delivery of DK14 chalcone analogue: A promising therapeutic strategy against triple-negative breast cancer
topic Biomedical and clinical sciences
Oncology and carcinogenesis
Pharmacology and pharmaceutical sciences
Anticancer
Apoptosis
Breast cancer
Chalcone analogue
Metastasis
Liposome