Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions

<p>Limited attention has been given to understanding how failure to the selective layer of reverse osmosis (RO) membranes develops and accumulates during operation; and to integrating this response into membrane fabrication. While the integrity of the selective layer is crucial for the separat...

وصف كامل

محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Abedalkader Alkhouzaam (15842647) (author)
مؤلفون آخرون: Fatima Ghassan Alabtah (15842650) (author), Marwan Khraisheh (15842653) (author)
منشور في: 2023
الموضوعات:
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author Abedalkader Alkhouzaam (15842647)
author2 Fatima Ghassan Alabtah (15842650)
Marwan Khraisheh (15842653)
author2_role author
author
author_facet Abedalkader Alkhouzaam (15842647)
Fatima Ghassan Alabtah (15842650)
Marwan Khraisheh (15842653)
author_role author
dc.creator.none.fl_str_mv Abedalkader Alkhouzaam (15842647)
Fatima Ghassan Alabtah (15842650)
Marwan Khraisheh (15842653)
dc.date.none.fl_str_mv 2023-07-01T00:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.surfin.2023.102911
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Evolution_of_surface_damage_of_thin_film_composite_TFC_reverse_osmosis_RO_membranes_under_controlled_hygro-mechanical_conditions/23092247
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Physical chemistry
Engineering
Mechanical engineering
Thin-film composite (TFC) membranes
Mechanical integrity
TFC stability
Surface characterization
Interrupted mechanical testing
dc.title.none.fl_str_mv Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p>Limited attention has been given to understanding how failure to the selective layer of reverse osmosis (RO) membranes develops and accumulates during operation; and to integrating this response into membrane fabrication. While the integrity of the selective layer is crucial for the separation process, available studies are limited to simple loading conditions and use failure of the entire membrane at rupture to represent its mechanical integrity. This work aims to investigate the evolution of surface damage to the selective layer under controlled interrupted mechanical tests under dry and wet conditions. AFM, SEM, and contact angle are used to characterize the selective layer integrity. Wet membranes exhibited lower strain at rupture (10.3%) than that of dry membranes (12.3%). However, interrupted tests revealed that the failure of the selective layer occurred at much lower strains than the rupture strain. Stretching and thinning in the TFC layer were observed at strain limits as low as 5%, which developed into localized deformation and cracks at higher strain limits (i.e., 8%). These findings can explain why membranes fail to perform before rupture occurs. By understanding how the selective layer's surface damage evolves during operation, membrane fabrication can be improved to enhance membrane performance and durability. </p> <h2>Other Information</h2> <p>Published in: Surfaces and Interfaces<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br> See article on publisher's website: <a href="https://doi.org/10.1016/j.surfin.2023.102911" target="_blank">https://doi.org/10.1016/j.surfin.2023.102911</a> </p>
eu_rights_str_mv openAccess
id Manara2_a67939c358193ccf2fdf6303b24126b8
identifier_str_mv 10.1016/j.surfin.2023.102911
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/23092247
publishDate 2023
repository.mail.fl_str_mv
repository.name.fl_str_mv
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rights_invalid_str_mv CC BY 4.0
spelling Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditionsAbedalkader Alkhouzaam (15842647)Fatima Ghassan Alabtah (15842650)Marwan Khraisheh (15842653)Chemical sciencesPhysical chemistryEngineeringMechanical engineeringThin-film composite (TFC) membranesMechanical integrityTFC stabilitySurface characterizationInterrupted mechanical testing<p>Limited attention has been given to understanding how failure to the selective layer of reverse osmosis (RO) membranes develops and accumulates during operation; and to integrating this response into membrane fabrication. While the integrity of the selective layer is crucial for the separation process, available studies are limited to simple loading conditions and use failure of the entire membrane at rupture to represent its mechanical integrity. This work aims to investigate the evolution of surface damage to the selective layer under controlled interrupted mechanical tests under dry and wet conditions. AFM, SEM, and contact angle are used to characterize the selective layer integrity. Wet membranes exhibited lower strain at rupture (10.3%) than that of dry membranes (12.3%). However, interrupted tests revealed that the failure of the selective layer occurred at much lower strains than the rupture strain. Stretching and thinning in the TFC layer were observed at strain limits as low as 5%, which developed into localized deformation and cracks at higher strain limits (i.e., 8%). These findings can explain why membranes fail to perform before rupture occurs. By understanding how the selective layer's surface damage evolves during operation, membrane fabrication can be improved to enhance membrane performance and durability. </p> <h2>Other Information</h2> <p>Published in: Surfaces and Interfaces<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br> See article on publisher's website: <a href="https://doi.org/10.1016/j.surfin.2023.102911" target="_blank">https://doi.org/10.1016/j.surfin.2023.102911</a> </p>2023-07-01T00:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.surfin.2023.102911https://figshare.com/articles/journal_contribution/Evolution_of_surface_damage_of_thin_film_composite_TFC_reverse_osmosis_RO_membranes_under_controlled_hygro-mechanical_conditions/23092247CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/230922472023-07-01T00:00:00Z
spellingShingle Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions
Abedalkader Alkhouzaam (15842647)
Chemical sciences
Physical chemistry
Engineering
Mechanical engineering
Thin-film composite (TFC) membranes
Mechanical integrity
TFC stability
Surface characterization
Interrupted mechanical testing
status_str publishedVersion
title Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions
title_full Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions
title_fullStr Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions
title_full_unstemmed Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions
title_short Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions
title_sort Evolution of surface damage of thin film composite (TFC) reverse osmosis (RO) membranes under controlled hygro-mechanical conditions
topic Chemical sciences
Physical chemistry
Engineering
Mechanical engineering
Thin-film composite (TFC) membranes
Mechanical integrity
TFC stability
Surface characterization
Interrupted mechanical testing