Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study

<p>In situ electrochemical microcantilever bending tests were conducted in this study to investigate the role of grain boundaries (GBs) in hydrogen embrittlement (HE) of Alloy 725. Specimens were prepared under three different heat treatment conditions and denoted as solution-annealed (SA), ag...

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محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Iman Taji (19457578) (author)
مؤلفون آخرون: Tarlan Hajilou (19457587) (author), Shabnam Karimi (19457575) (author), Florian Schott (19517434) (author), Ernst Plesiutschnig (19517437) (author), Afrooz Barnoush (7410176) (author), Roy Johnsen (19457590) (author)
منشور في: 2022
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author Iman Taji (19457578)
author2 Tarlan Hajilou (19457587)
Shabnam Karimi (19457575)
Florian Schott (19517434)
Ernst Plesiutschnig (19517437)
Afrooz Barnoush (7410176)
Roy Johnsen (19457590)
author2_role author
author
author
author
author
author
author_facet Iman Taji (19457578)
Tarlan Hajilou (19457587)
Shabnam Karimi (19457575)
Florian Schott (19517434)
Ernst Plesiutschnig (19517437)
Afrooz Barnoush (7410176)
Roy Johnsen (19457590)
author_role author
dc.creator.none.fl_str_mv Iman Taji (19457578)
Tarlan Hajilou (19457587)
Shabnam Karimi (19457575)
Florian Schott (19517434)
Ernst Plesiutschnig (19517437)
Afrooz Barnoush (7410176)
Roy Johnsen (19457590)
dc.date.none.fl_str_mv 2022-03-14T09:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.ijhydene.2022.01.251
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Role_of_grain_boundaries_in_hydrogen_embrittlement_of_alloy_725_single_and_bi-crystal_microcantilever_bending_study/26889097
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Physical chemistry
Microcantilever bending
Alloy 725Heat treatment
Hydrogen embrittlement
Grain boundary
dc.title.none.fl_str_mv Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p>In situ electrochemical microcantilever bending tests were conducted in this study to investigate the role of grain boundaries (GBs) in hydrogen embrittlement (HE) of Alloy 725. Specimens were prepared under three different heat treatment conditions and denoted as solution-annealed (SA), aged (AG) and over-aged (OA) samples. For single-crystal beams in an H-containing environment, all three heat-treated samples exhibited crack formation and propagation; however, crack propagation was more severe in the OA sample. The anodic extraction of H presented similar results as those under the H-free condition, indicating the reversibility of the H effect under the tested conditions. Bi-crystal micro-cantilevers bent under H-free and H-charged conditions revealed the significant role of the GB in the HE of the beams. The results indicated that the GB in the SA sample facilitated dislocation dissipation, whereas for the OA sample, it caused the retardation of crack propagation. For the AG sample, testing in an H-containing environment led to the formation of a sharp, severe crack along the GB path.</p><h2>Other Information</h2> <p> Published in: International Journal of Hydrogen Energy<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.ijhydene.2022.01.251" target="_blank">https://dx.doi.org/10.1016/j.ijhydene.2022.01.251</a></p>
eu_rights_str_mv openAccess
id Manara2_a93c92ef3b25195c82e40ca0492f7e6e
identifier_str_mv 10.1016/j.ijhydene.2022.01.251
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/26889097
publishDate 2022
repository.mail.fl_str_mv
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rights_invalid_str_mv CC BY 4.0
spelling Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending studyIman Taji (19457578)Tarlan Hajilou (19457587)Shabnam Karimi (19457575)Florian Schott (19517434)Ernst Plesiutschnig (19517437)Afrooz Barnoush (7410176)Roy Johnsen (19457590)Chemical sciencesPhysical chemistryMicrocantilever bendingAlloy 725Heat treatmentHydrogen embrittlementGrain boundary<p>In situ electrochemical microcantilever bending tests were conducted in this study to investigate the role of grain boundaries (GBs) in hydrogen embrittlement (HE) of Alloy 725. Specimens were prepared under three different heat treatment conditions and denoted as solution-annealed (SA), aged (AG) and over-aged (OA) samples. For single-crystal beams in an H-containing environment, all three heat-treated samples exhibited crack formation and propagation; however, crack propagation was more severe in the OA sample. The anodic extraction of H presented similar results as those under the H-free condition, indicating the reversibility of the H effect under the tested conditions. Bi-crystal micro-cantilevers bent under H-free and H-charged conditions revealed the significant role of the GB in the HE of the beams. The results indicated that the GB in the SA sample facilitated dislocation dissipation, whereas for the OA sample, it caused the retardation of crack propagation. For the AG sample, testing in an H-containing environment led to the formation of a sharp, severe crack along the GB path.</p><h2>Other Information</h2> <p> Published in: International Journal of Hydrogen Energy<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.ijhydene.2022.01.251" target="_blank">https://dx.doi.org/10.1016/j.ijhydene.2022.01.251</a></p>2022-03-14T09:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.ijhydene.2022.01.251https://figshare.com/articles/journal_contribution/Role_of_grain_boundaries_in_hydrogen_embrittlement_of_alloy_725_single_and_bi-crystal_microcantilever_bending_study/26889097CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/268890972022-03-14T09:00:00Z
spellingShingle Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study
Iman Taji (19457578)
Chemical sciences
Physical chemistry
Microcantilever bending
Alloy 725Heat treatment
Hydrogen embrittlement
Grain boundary
status_str publishedVersion
title Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study
title_full Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study
title_fullStr Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study
title_full_unstemmed Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study
title_short Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study
title_sort Role of grain boundaries in hydrogen embrittlement of alloy 725: single and bi-crystal microcantilever bending study
topic Chemical sciences
Physical chemistry
Microcantilever bending
Alloy 725Heat treatment
Hydrogen embrittlement
Grain boundary