Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells

<p dir="ltr">Nb-doped SrFeO<sub>3−</sub><sub><em>δ</em></sub> (SFO) is used as a cathode in proton-conducting solid oxide fuel cells (H-SOFCs). First-principles calculations show that the SrFe<sub>0.9</sub>Nb<sub>0.1</sub>O&...

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Main Author: Hailu Dai (19239613) (author)
Other Authors: Hongzhe Du (11955738) (author), Samir Boulfrad (17823419) (author), Shoufu Yu (19239616) (author), Lei Bi (1944472) (author), Qinfang Zhang (5491889) (author)
Published: 2024
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_version_ 1864513510162038784
author Hailu Dai (19239613)
author2 Hongzhe Du (11955738)
Samir Boulfrad (17823419)
Shoufu Yu (19239616)
Lei Bi (1944472)
Qinfang Zhang (5491889)
author2_role author
author
author
author
author
author_facet Hailu Dai (19239613)
Hongzhe Du (11955738)
Samir Boulfrad (17823419)
Shoufu Yu (19239616)
Lei Bi (1944472)
Qinfang Zhang (5491889)
author_role author
dc.creator.none.fl_str_mv Hailu Dai (19239613)
Hongzhe Du (11955738)
Samir Boulfrad (17823419)
Shoufu Yu (19239616)
Lei Bi (1944472)
Qinfang Zhang (5491889)
dc.date.none.fl_str_mv 2024-03-18T12:00:00Z
dc.identifier.none.fl_str_mv 10.26599/jac.2024.9220880
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Manipulating_Nb-doped_SrFeO_sub_3_sub_sub_em_em_sub_with_excellent_performance_for_proton-conducting_solid_oxide_fuel_cells/26392867
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Engineering
Materials engineering
SrFeO3−δ (SFO)
cathode
proton conductor
solid oxide fuel cells (SOFCs)
dc.title.none.fl_str_mv Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">Nb-doped SrFeO<sub>3−</sub><sub><em>δ</em></sub> (SFO) is used as a cathode in proton-conducting solid oxide fuel cells (H-SOFCs). First-principles calculations show that the SrFe<sub>0.9</sub>Nb<sub>0.1</sub>O<sub>3−</sub><sub><em>δ</em></sub> (SFNO) cathode has a lower energy barrier in the cathode reaction for H-SOFCs than the Nb-free SrFeO<sub>3−</sub><sub><em>δ</em></sub> cathode. Subsequent experimental studies show that Nb doping substantially enhances the performance of the SrFeO<sub>3−</sub><sub><em>δ</em></sub> cathode. Then, oxygen vacancies (V<sub>O</sub>) were introduced into SFNO using the microwave sintering method, further improving the performance of the SFNO cathode. The mechanism behind the performance improvement owing to V<sub>O</sub> was revealed using first-principles calculations, with further optimization of the SFNO cathode achieved by developing a suitable wet chemical synthesis route to prepare nanosized SFNO materials. This method significantly reduces the grain size of SFNO compared with the conventional solid-state reaction method, although the solid-state reaction method is generally used for preparing Nb-containing oxides. As a result of defect engineering and synthesis approaches, the SFNO cathode achieved an attractive fuel cell performance, attaining an output of 1764 mW·cm<sup>−2</sup> at 700 °C and operating for more than 200 h. The manipulation of Nb-doped SrFeO<sub>3−</sub><sub><em>δ</em></sub> can be seen as a “one stone, two birds” strategy, enhancing cathode performance while retaining good stability, thus providing an interesting approach for constructing high-performance cathodes for H-SOFCs.</p><h2>Other Information</h2><p dir="ltr">Published in: Journal of Advanced Ceramics<br>License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.26599/jac.2024.9220880" target="_blank">https://dx.doi.org/10.26599/jac.2024.9220880</a></p>
eu_rights_str_mv openAccess
id Manara2_b969d99d34c21258577acc5de51d0e30
identifier_str_mv 10.26599/jac.2024.9220880
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/26392867
publishDate 2024
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rights_invalid_str_mv CC BY 4.0
spelling Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cellsHailu Dai (19239613)Hongzhe Du (11955738)Samir Boulfrad (17823419)Shoufu Yu (19239616)Lei Bi (1944472)Qinfang Zhang (5491889)EngineeringMaterials engineeringSrFeO3−δ (SFO)cathodeproton conductorsolid oxide fuel cells (SOFCs)<p dir="ltr">Nb-doped SrFeO<sub>3−</sub><sub><em>δ</em></sub> (SFO) is used as a cathode in proton-conducting solid oxide fuel cells (H-SOFCs). First-principles calculations show that the SrFe<sub>0.9</sub>Nb<sub>0.1</sub>O<sub>3−</sub><sub><em>δ</em></sub> (SFNO) cathode has a lower energy barrier in the cathode reaction for H-SOFCs than the Nb-free SrFeO<sub>3−</sub><sub><em>δ</em></sub> cathode. Subsequent experimental studies show that Nb doping substantially enhances the performance of the SrFeO<sub>3−</sub><sub><em>δ</em></sub> cathode. Then, oxygen vacancies (V<sub>O</sub>) were introduced into SFNO using the microwave sintering method, further improving the performance of the SFNO cathode. The mechanism behind the performance improvement owing to V<sub>O</sub> was revealed using first-principles calculations, with further optimization of the SFNO cathode achieved by developing a suitable wet chemical synthesis route to prepare nanosized SFNO materials. This method significantly reduces the grain size of SFNO compared with the conventional solid-state reaction method, although the solid-state reaction method is generally used for preparing Nb-containing oxides. As a result of defect engineering and synthesis approaches, the SFNO cathode achieved an attractive fuel cell performance, attaining an output of 1764 mW·cm<sup>−2</sup> at 700 °C and operating for more than 200 h. The manipulation of Nb-doped SrFeO<sub>3−</sub><sub><em>δ</em></sub> can be seen as a “one stone, two birds” strategy, enhancing cathode performance while retaining good stability, thus providing an interesting approach for constructing high-performance cathodes for H-SOFCs.</p><h2>Other Information</h2><p dir="ltr">Published in: Journal of Advanced Ceramics<br>License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.26599/jac.2024.9220880" target="_blank">https://dx.doi.org/10.26599/jac.2024.9220880</a></p>2024-03-18T12:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.26599/jac.2024.9220880https://figshare.com/articles/journal_contribution/Manipulating_Nb-doped_SrFeO_sub_3_sub_sub_em_em_sub_with_excellent_performance_for_proton-conducting_solid_oxide_fuel_cells/26392867CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/263928672024-03-18T12:00:00Z
spellingShingle Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells
Hailu Dai (19239613)
Engineering
Materials engineering
SrFeO3−δ (SFO)
cathode
proton conductor
solid oxide fuel cells (SOFCs)
status_str publishedVersion
title Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells
title_full Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells
title_fullStr Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells
title_full_unstemmed Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells
title_short Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells
title_sort Manipulating Nb-doped SrFeO <sub>3− </sub><sub><em>δ </em></sub>with excellent performance for proton-conducting solid oxide fuel cells
topic Engineering
Materials engineering
SrFeO3−δ (SFO)
cathode
proton conductor
solid oxide fuel cells (SOFCs)