Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications

<div><p>Anion exchange membranes (AEMs) are becoming increasingly common in electrochemical energy conversion and storage systems around the world (EES). Proton-/cation-exchange membranes (which conduct positive charged ions such as H+ or Na+) have historically been used in many devices...

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المؤلف الرئيسي: Muthumeenal Arunachalam (11450796) (author)
مؤلفون آخرون: Alessandro Sinopoli (4318555) (author), Farida Aidoudi (11450799) (author), Stephen E. Creager (2038834) (author), Rhett Smith (11450802) (author), Belabbes Merzougui (4724322) (author), Brahim Aïssa (14157243) (author)
منشور في: 2021
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author Muthumeenal Arunachalam (11450796)
author2 Alessandro Sinopoli (4318555)
Farida Aidoudi (11450799)
Stephen E. Creager (2038834)
Rhett Smith (11450802)
Belabbes Merzougui (4724322)
Brahim Aïssa (14157243)
author2_role author
author
author
author
author
author
author_facet Muthumeenal Arunachalam (11450796)
Alessandro Sinopoli (4318555)
Farida Aidoudi (11450799)
Stephen E. Creager (2038834)
Rhett Smith (11450802)
Belabbes Merzougui (4724322)
Brahim Aïssa (14157243)
author_role author
dc.creator.none.fl_str_mv Muthumeenal Arunachalam (11450796)
Alessandro Sinopoli (4318555)
Farida Aidoudi (11450799)
Stephen E. Creager (2038834)
Rhett Smith (11450802)
Belabbes Merzougui (4724322)
Brahim Aïssa (14157243)
dc.date.none.fl_str_mv 2021-07-05T03:00:00Z
dc.identifier.none.fl_str_mv 10.1038/s41598-021-93273-x
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Investigating_the_suitability_of_poly_tetraarylphosphonium_based_anion_exchange_membranes_for_electrochemical_applications/25779804
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Macromolecular and materials chemistry
Engineering
Materials engineering
Fuel cells
Electrolysers
Redox flow batteries
Polymer electrolyte membrane (PEM)
Noble metal catalysts
Alkaline environment
Non-precious metals
dc.title.none.fl_str_mv Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <div><p>Anion exchange membranes (AEMs) are becoming increasingly common in electrochemical energy conversion and storage systems around the world (EES). Proton-/cation-exchange membranes (which conduct positive charged ions such as H+ or Na+) have historically been used in many devices such as fuel cells, electrolysers, and redox flow batteries. High capital costs and the use of noble metal catalysts are two of the current major disadvantages of polymer electrolyte membrane (PEM)-based systems. AEMs may be able to overcome the limitations of conventional PEMs. As a result, polymers with anion exchange properties have recently attracted a lot of attention due to their significant benefits in terms of transitioning from a highly acidic to an alkaline environment, high kinetics for oxygen reduction and fuel oxidation in an alkaline environment, and lower cost due to the use of non-precious metals. The aim of this research was to learn more about the development of a new AEM based on poly tetraarylphosphonium ionomers (pTAP), which has high ionic conductivity, alkaline stability, thermal stability, and good mechanical properties, making it a more cost-effective and stable alternative to conventional and commercial AEMs. A simple solution casting method was used to build novel anion exchange composite membranes with controlled thicknesses using the synthesized pTAP with polysulfone (PS). To ensure their suitability for use as an electrolyte in alkaline electrochemical systems, the composite membranes were characterized using FTIR, XRD, water uptake, ionic conductivity, and alkaline stability. At 40 °C, the PS/pTAP 40/60 percent membrane had a maximum ionic conductivity of 4.2 mS/cm. The thermal and mechanical stability of the composite membranes were also examined, with no substantial weight loss observed up to 150 °C. These findings pave the way for these membranes to be used in a wide variety of electrochemical applications.</p><p> </p></div><h2>Other Information</h2> <p> Published in: Scientific Reports<br> License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1038/s41598-021-93273-x" target="_blank">https://dx.doi.org/10.1038/s41598-021-93273-x</a></p>
eu_rights_str_mv openAccess
id Manara2_c3e6572bb4a7dfd5298e89be59bc06ec
identifier_str_mv 10.1038/s41598-021-93273-x
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/25779804
publishDate 2021
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spelling Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applicationsMuthumeenal Arunachalam (11450796)Alessandro Sinopoli (4318555)Farida Aidoudi (11450799)Stephen E. Creager (2038834)Rhett Smith (11450802)Belabbes Merzougui (4724322)Brahim Aïssa (14157243)Chemical sciencesMacromolecular and materials chemistryEngineeringMaterials engineeringFuel cellsElectrolysersRedox flow batteriesPolymer electrolyte membrane (PEM)Noble metal catalystsAlkaline environmentNon-precious metals<div><p>Anion exchange membranes (AEMs) are becoming increasingly common in electrochemical energy conversion and storage systems around the world (EES). Proton-/cation-exchange membranes (which conduct positive charged ions such as H+ or Na+) have historically been used in many devices such as fuel cells, electrolysers, and redox flow batteries. High capital costs and the use of noble metal catalysts are two of the current major disadvantages of polymer electrolyte membrane (PEM)-based systems. AEMs may be able to overcome the limitations of conventional PEMs. As a result, polymers with anion exchange properties have recently attracted a lot of attention due to their significant benefits in terms of transitioning from a highly acidic to an alkaline environment, high kinetics for oxygen reduction and fuel oxidation in an alkaline environment, and lower cost due to the use of non-precious metals. The aim of this research was to learn more about the development of a new AEM based on poly tetraarylphosphonium ionomers (pTAP), which has high ionic conductivity, alkaline stability, thermal stability, and good mechanical properties, making it a more cost-effective and stable alternative to conventional and commercial AEMs. A simple solution casting method was used to build novel anion exchange composite membranes with controlled thicknesses using the synthesized pTAP with polysulfone (PS). To ensure their suitability for use as an electrolyte in alkaline electrochemical systems, the composite membranes were characterized using FTIR, XRD, water uptake, ionic conductivity, and alkaline stability. At 40 °C, the PS/pTAP 40/60 percent membrane had a maximum ionic conductivity of 4.2 mS/cm. The thermal and mechanical stability of the composite membranes were also examined, with no substantial weight loss observed up to 150 °C. These findings pave the way for these membranes to be used in a wide variety of electrochemical applications.</p><p> </p></div><h2>Other Information</h2> <p> Published in: Scientific Reports<br> License: <a href="https://creativecommons.org/licenses/by/4.0" target="_blank">https://creativecommons.org/licenses/by/4.0</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1038/s41598-021-93273-x" target="_blank">https://dx.doi.org/10.1038/s41598-021-93273-x</a></p>2021-07-05T03:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1038/s41598-021-93273-xhttps://figshare.com/articles/journal_contribution/Investigating_the_suitability_of_poly_tetraarylphosphonium_based_anion_exchange_membranes_for_electrochemical_applications/25779804CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/257798042021-07-05T03:00:00Z
spellingShingle Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications
Muthumeenal Arunachalam (11450796)
Chemical sciences
Macromolecular and materials chemistry
Engineering
Materials engineering
Fuel cells
Electrolysers
Redox flow batteries
Polymer electrolyte membrane (PEM)
Noble metal catalysts
Alkaline environment
Non-precious metals
status_str publishedVersion
title Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications
title_full Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications
title_fullStr Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications
title_full_unstemmed Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications
title_short Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications
title_sort Investigating the suitability of poly tetraarylphosphonium based anion exchange membranes for electrochemical applications
topic Chemical sciences
Macromolecular and materials chemistry
Engineering
Materials engineering
Fuel cells
Electrolysers
Redox flow batteries
Polymer electrolyte membrane (PEM)
Noble metal catalysts
Alkaline environment
Non-precious metals