Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors

<p dir="ltr">We employ a fine-tuned theoretical framework, combining ab initio molecular dynamics (AIMD), density functional theory (DFT), and time-dependent (TD) DFT methods, to investigate the interactions and optical properties of the iodoplumbates within the low coordinative γ-bu...

وصف كامل

محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Eros Radicchi (3757978) (author)
مؤلفون آخرون: Ali Kachmar (1609192) (author), Edoardo Mosconi (1305621) (author), Beatrice Bizzarri (9142295) (author), Francesca Nunzi (1659013) (author), Filippo De Angelis (7246292) (author)
منشور في: 2020
الموضوعات:
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author Eros Radicchi (3757978)
author2 Ali Kachmar (1609192)
Edoardo Mosconi (1305621)
Beatrice Bizzarri (9142295)
Francesca Nunzi (1659013)
Filippo De Angelis (7246292)
author2_role author
author
author
author
author
author_facet Eros Radicchi (3757978)
Ali Kachmar (1609192)
Edoardo Mosconi (1305621)
Beatrice Bizzarri (9142295)
Francesca Nunzi (1659013)
Filippo De Angelis (7246292)
author_role author
dc.creator.none.fl_str_mv Eros Radicchi (3757978)
Ali Kachmar (1609192)
Edoardo Mosconi (1305621)
Beatrice Bizzarri (9142295)
Francesca Nunzi (1659013)
Filippo De Angelis (7246292)
dc.date.none.fl_str_mv 2020-07-09T03:00:00Z
dc.identifier.none.fl_str_mv 10.1021/acs.jpclett.0c01890
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Structural_and_Optical_Properties_of_Solvated_PbI_sub_2_sub_in_-Butyrolactone_Insight_into_the_Solution_Chemistry_of_Lead_Halide_Perovskite_Precursors/25808725
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Chemical sciences
Theoretical and computational chemistry
Engineering
Materials engineering
Lead-halide perovskites
Optoelectronic properties
Solution synthesis
Thin film deposition
Solvent engineering
Power conversion efficiency
Perovskite morphology
dc.title.none.fl_str_mv Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">We employ a fine-tuned theoretical framework, combining ab initio molecular dynamics (AIMD), density functional theory (DFT), and time-dependent (TD) DFT methods, to investigate the interactions and optical properties of the iodoplumbates within the low coordinative γ-butyrolactone (GBL) solvent environment, widely employed in the perovskite synthesis. We uncover the extent of GBL coordination to PbI2 investigating its relation to the solvated PbI2 optical properties. The employed approach has been further validated by comparison with the experimental UV–vis absorption spectrum of PbI2 in GBL solvent. A comparison with other solvents, commonly employed in the perovskite synthesis, such as N,N-dimethylformamide (DMF) and dimethyl sulfoxide (DMSO) is also reported. The methodology developed in this work can be reasonably extended to the investigation of similar systems.</p><h2>Other Information</h2><p dir="ltr">Published in: The Journal of Physical Chemistry Letters<br>License: <a href="https://creativecommons.org/licenses/by/4.0/" target="_blank">https://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1021/acs.jpclett.0c01890" target="_blank">https://dx.doi.org/10.1021/acs.jpclett.0c01890</a></p>
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id Manara2_c5e8fed299594bb60a74e4b7ecd9d8ca
identifier_str_mv 10.1021/acs.jpclett.0c01890
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/25808725
publishDate 2020
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rights_invalid_str_mv CC BY 4.0
spelling Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite PrecursorsEros Radicchi (3757978)Ali Kachmar (1609192)Edoardo Mosconi (1305621)Beatrice Bizzarri (9142295)Francesca Nunzi (1659013)Filippo De Angelis (7246292)Chemical sciencesTheoretical and computational chemistryEngineeringMaterials engineeringLead-halide perovskitesOptoelectronic propertiesSolution synthesisThin film depositionSolvent engineeringPower conversion efficiencyPerovskite morphology<p dir="ltr">We employ a fine-tuned theoretical framework, combining ab initio molecular dynamics (AIMD), density functional theory (DFT), and time-dependent (TD) DFT methods, to investigate the interactions and optical properties of the iodoplumbates within the low coordinative γ-butyrolactone (GBL) solvent environment, widely employed in the perovskite synthesis. We uncover the extent of GBL coordination to PbI2 investigating its relation to the solvated PbI2 optical properties. The employed approach has been further validated by comparison with the experimental UV–vis absorption spectrum of PbI2 in GBL solvent. A comparison with other solvents, commonly employed in the perovskite synthesis, such as N,N-dimethylformamide (DMF) and dimethyl sulfoxide (DMSO) is also reported. The methodology developed in this work can be reasonably extended to the investigation of similar systems.</p><h2>Other Information</h2><p dir="ltr">Published in: The Journal of Physical Chemistry Letters<br>License: <a href="https://creativecommons.org/licenses/by/4.0/" target="_blank">https://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1021/acs.jpclett.0c01890" target="_blank">https://dx.doi.org/10.1021/acs.jpclett.0c01890</a></p>2020-07-09T03:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1021/acs.jpclett.0c01890https://figshare.com/articles/journal_contribution/Structural_and_Optical_Properties_of_Solvated_PbI_sub_2_sub_in_-Butyrolactone_Insight_into_the_Solution_Chemistry_of_Lead_Halide_Perovskite_Precursors/25808725CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/258087252020-07-09T03:00:00Z
spellingShingle Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors
Eros Radicchi (3757978)
Chemical sciences
Theoretical and computational chemistry
Engineering
Materials engineering
Lead-halide perovskites
Optoelectronic properties
Solution synthesis
Thin film deposition
Solvent engineering
Power conversion efficiency
Perovskite morphology
status_str publishedVersion
title Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors
title_full Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors
title_fullStr Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors
title_full_unstemmed Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors
title_short Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors
title_sort Structural and Optical Properties of Solvated PbI<sub>2</sub> in γ-Butyrolactone: Insight into the Solution Chemistry of Lead Halide Perovskite Precursors
topic Chemical sciences
Theoretical and computational chemistry
Engineering
Materials engineering
Lead-halide perovskites
Optoelectronic properties
Solution synthesis
Thin film deposition
Solvent engineering
Power conversion efficiency
Perovskite morphology