Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing

<p dir="ltr">In this study, we developed nanocomposite films from a blend of Polyvinylidene Fluoride (PVDF) and Polyethylene Glycol (PEG), incorporating varying concentrations of Zinc Oxide (ZnO) and Barium Titanate (BaTiO₃) nanoparticles. PVDF/PEG based films were prepared via the n...

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محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Maryam Al-Ejji (5244842) (author)
مؤلفون آخرون: Rayane Akoumeh (18560659) (author), Taghreed Alsulami (22997824) (author), Farah Sangor (22997827) (author), Zinab Al-Awa (22997830) (author), Khadija Zadeh (22997833) (author), Deepalekshmi Ponnamma (1389270) (author)
منشور في: 2025
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_version_ 1864513524517044224
author Maryam Al-Ejji (5244842)
author2 Rayane Akoumeh (18560659)
Taghreed Alsulami (22997824)
Farah Sangor (22997827)
Zinab Al-Awa (22997830)
Khadija Zadeh (22997833)
Deepalekshmi Ponnamma (1389270)
author2_role author
author
author
author
author
author
author_facet Maryam Al-Ejji (5244842)
Rayane Akoumeh (18560659)
Taghreed Alsulami (22997824)
Farah Sangor (22997827)
Zinab Al-Awa (22997830)
Khadija Zadeh (22997833)
Deepalekshmi Ponnamma (1389270)
author_role author
dc.creator.none.fl_str_mv Maryam Al-Ejji (5244842)
Rayane Akoumeh (18560659)
Taghreed Alsulami (22997824)
Farah Sangor (22997827)
Zinab Al-Awa (22997830)
Khadija Zadeh (22997833)
Deepalekshmi Ponnamma (1389270)
dc.date.none.fl_str_mv 2025-09-16T15:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.mtcomm.2025.113756
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Enhancing_piezoelectric_performance_of_PVDF_PEG_blends_with_ZnO_and_BaTiO_nanofillers_for_nanogenerator_and_UV_sensing/31056973
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Engineering
Materials engineering
Nanotechnology
Piezoelectric Sensing
PVDF/PEG Nanocomposites
Non-solvent Induced Phase Separation
Nanomaterials
Surface Wettability
dc.title.none.fl_str_mv Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p dir="ltr">In this study, we developed nanocomposite films from a blend of Polyvinylidene Fluoride (PVDF) and Polyethylene Glycol (PEG), incorporating varying concentrations of Zinc Oxide (ZnO) and Barium Titanate (BaTiO₃) nanoparticles. PVDF/PEG based films were prepared via the non-solvent induced phase separation (NIPS) technique to achieve simultaneous multifunctional properties for nanogeneration and UV sensing, a dual functionality rarely reported. The ZnO nanoparticles exhibit a colloidal morphology with an average size of 27.04 ± 0.7 nm, while BaTiO₃ nanoparticles exhibit a cubic shaped with an average size of 67.84 ± 1.7 nm. The pristine polymer nanocomposite membrane exhibited slight irregular porosity (>1 µm, 19.82 %), which increased upon incorporation of nanoparticles. With 0.5 and 1 wt% of nanofillers, the membranes displayed heterogeneous pore structures ranging from 200 nm to 4 µm, and porosity of 21.42 % and 24.11 %, respectively. Surface wettability analysis indicates that all films were highly hydrophobic, with contact angles exceeding 110°, attributed to the inherent hydrophobic nature of PVDF/PEG blend and surface roughness. The optimal output voltage and UV sensing were observed at low nanoparticle concentration, with a peak-to-peak voltage of 1.4 V for 0.5 wt% of the ZnO/BaTiO<sub>3</sub>. However, nanoparticle concentrations above 3 wt% lead to a reduction in both the PVDF/PEG crystallinity (Xc) and the β-phase fraction. The fine-tuning of nanoparticle content enhances the piezoelectric properties of the nanocomposite PVDF/PEG film.</p><h2 dir="ltr">Other Information</h2><p dir="ltr">Published in: Materials Today Communications<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.mtcomm.2025.113756" target="_blank">https://dx.doi.org/10.1016/j.mtcomm.2025.113756</a></p>
eu_rights_str_mv openAccess
id Manara2_ceb1b83f7a3ecd021fcb3ba473a848bd
identifier_str_mv 10.1016/j.mtcomm.2025.113756
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/31056973
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rights_invalid_str_mv CC BY 4.0
spelling Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensingMaryam Al-Ejji (5244842)Rayane Akoumeh (18560659)Taghreed Alsulami (22997824)Farah Sangor (22997827)Zinab Al-Awa (22997830)Khadija Zadeh (22997833)Deepalekshmi Ponnamma (1389270)EngineeringMaterials engineeringNanotechnologyPiezoelectric SensingPVDF/PEG NanocompositesNon-solvent Induced Phase SeparationNanomaterialsSurface Wettability<p dir="ltr">In this study, we developed nanocomposite films from a blend of Polyvinylidene Fluoride (PVDF) and Polyethylene Glycol (PEG), incorporating varying concentrations of Zinc Oxide (ZnO) and Barium Titanate (BaTiO₃) nanoparticles. PVDF/PEG based films were prepared via the non-solvent induced phase separation (NIPS) technique to achieve simultaneous multifunctional properties for nanogeneration and UV sensing, a dual functionality rarely reported. The ZnO nanoparticles exhibit a colloidal morphology with an average size of 27.04 ± 0.7 nm, while BaTiO₃ nanoparticles exhibit a cubic shaped with an average size of 67.84 ± 1.7 nm. The pristine polymer nanocomposite membrane exhibited slight irregular porosity (>1 µm, 19.82 %), which increased upon incorporation of nanoparticles. With 0.5 and 1 wt% of nanofillers, the membranes displayed heterogeneous pore structures ranging from 200 nm to 4 µm, and porosity of 21.42 % and 24.11 %, respectively. Surface wettability analysis indicates that all films were highly hydrophobic, with contact angles exceeding 110°, attributed to the inherent hydrophobic nature of PVDF/PEG blend and surface roughness. The optimal output voltage and UV sensing were observed at low nanoparticle concentration, with a peak-to-peak voltage of 1.4 V for 0.5 wt% of the ZnO/BaTiO<sub>3</sub>. However, nanoparticle concentrations above 3 wt% lead to a reduction in both the PVDF/PEG crystallinity (Xc) and the β-phase fraction. The fine-tuning of nanoparticle content enhances the piezoelectric properties of the nanocomposite PVDF/PEG film.</p><h2 dir="ltr">Other Information</h2><p dir="ltr">Published in: Materials Today Communications<br>License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.mtcomm.2025.113756" target="_blank">https://dx.doi.org/10.1016/j.mtcomm.2025.113756</a></p>2025-09-16T15:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.mtcomm.2025.113756https://figshare.com/articles/journal_contribution/Enhancing_piezoelectric_performance_of_PVDF_PEG_blends_with_ZnO_and_BaTiO_nanofillers_for_nanogenerator_and_UV_sensing/31056973CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/310569732025-09-16T15:00:00Z
spellingShingle Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing
Maryam Al-Ejji (5244842)
Engineering
Materials engineering
Nanotechnology
Piezoelectric Sensing
PVDF/PEG Nanocomposites
Non-solvent Induced Phase Separation
Nanomaterials
Surface Wettability
status_str publishedVersion
title Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing
title_full Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing
title_fullStr Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing
title_full_unstemmed Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing
title_short Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing
title_sort Enhancing piezoelectric performance of PVDF/PEG blends with ZnO and BaTiO₃ nanofillers for nanogenerator and UV sensing
topic Engineering
Materials engineering
Nanotechnology
Piezoelectric Sensing
PVDF/PEG Nanocomposites
Non-solvent Induced Phase Separation
Nanomaterials
Surface Wettability