Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles

<p>Silver-doped magnesia nanoparticles (Ag/MgO) were synthesized using the precipitation method and characterized by various techniques such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermal gravimetric analysis (TGA), Brunner-Emmett-Teller (BET) surface area...

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Main Author: Mohamed Qasim Al-Fahdawi (17844209) (author)
Other Authors: Ahmed Faris Aldoghachi (16301714) (author), Fatah H. Alhassan (17844212) (author), Faris A.J. Al-Doghachi (17844215) (author), Hussah Abdullah Alshwyeh (16621140) (author), Abdullah Rasedee (6940799) (author), Sulaiman Mohammed Alnasser (16713520) (author), Mothanna Sadiq Al-Qubaisi (17844218) (author), Wisam Nabeel Ibrahim (13899337) (author)
Published: 2023
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author Mohamed Qasim Al-Fahdawi (17844209)
author2 Ahmed Faris Aldoghachi (16301714)
Fatah H. Alhassan (17844212)
Faris A.J. Al-Doghachi (17844215)
Hussah Abdullah Alshwyeh (16621140)
Abdullah Rasedee (6940799)
Sulaiman Mohammed Alnasser (16713520)
Mothanna Sadiq Al-Qubaisi (17844218)
Wisam Nabeel Ibrahim (13899337)
author2_role author
author
author
author
author
author
author
author
author_facet Mohamed Qasim Al-Fahdawi (17844209)
Ahmed Faris Aldoghachi (16301714)
Fatah H. Alhassan (17844212)
Faris A.J. Al-Doghachi (17844215)
Hussah Abdullah Alshwyeh (16621140)
Abdullah Rasedee (6940799)
Sulaiman Mohammed Alnasser (16713520)
Mothanna Sadiq Al-Qubaisi (17844218)
Wisam Nabeel Ibrahim (13899337)
author_role author
dc.creator.none.fl_str_mv Mohamed Qasim Al-Fahdawi (17844209)
Ahmed Faris Aldoghachi (16301714)
Fatah H. Alhassan (17844212)
Faris A.J. Al-Doghachi (17844215)
Hussah Abdullah Alshwyeh (16621140)
Abdullah Rasedee (6940799)
Sulaiman Mohammed Alnasser (16713520)
Mothanna Sadiq Al-Qubaisi (17844218)
Wisam Nabeel Ibrahim (13899337)
dc.date.none.fl_str_mv 2023-04-17T03:00:00Z
dc.identifier.none.fl_str_mv 10.1016/j.heliyon.2023.e15560
dc.relation.none.fl_str_mv https://figshare.com/articles/journal_contribution/Physicochemical_characterization_and_cancer_cell_antiproliferative_effect_of_silver-doped_magnesia_nanoparticles/25059731
dc.rights.none.fl_str_mv CC BY 4.0
info:eu-repo/semantics/openAccess
dc.subject.none.fl_str_mv Biomedical and clinical sciences
Clinical sciences
Pharmacology and pharmaceutical sciences
Ag/MgO nanoparticles
HT29 cell
A549 cell
Antiproliferative
Apoptosis
dc.title.none.fl_str_mv Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles
dc.type.none.fl_str_mv Text
Journal contribution
info:eu-repo/semantics/publishedVersion
text
contribution to journal
description <p>Silver-doped magnesia nanoparticles (Ag/MgO) were synthesized using the precipitation method and characterized by various techniques such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermal gravimetric analysis (TGA), Brunner-Emmett-Teller (BET) surface area measurements, and dispersive X-ray spectroscopy (EDX). The morphology of Ag/MgO nanoparticles was determined by transmission and scanning electron microscopy, which revealed cuboidal shaped nanoparticles with sizes ranging from 31 to 68 nm and an average size of 43.5 ± 10.6 nm. The anticancer effects of Ag/MgO nanoparticles were evaluated on human colorectal (HT29) and lung adenocarcinoma (A549) cell lines, and their caspase-3, -8, and -9 activities, as well as Bcl-2, Bax, p53, cytochrome C protein expressions were estimated. Ag/MgO nanoparticles showed selective toxicity towards HT29 and A549 cells while remaining relatively innocuous towards the normal human colorectal, CCD-18Co, and lung, MRC-5 cells. The IC50 values of Ag/MgO nanoparticles on the HT29 and A549 cells were found to be 90.2 ± 2.6 and 85.0 ± 3.5 μg/mL, respectively. The Ag/MgO nanoparticles upregulated caspase-3 and -9 activities, downregulated Bcl-2, upregulated Bax and p53 protein expressions in the cancer cells. The morphology of the Ag/MgO nanoparticle treated HT29 and A549 cells was typical of apoptosis, with cell detachment, shrinkage, and membrane blebbing. The results suggest that Ag/MgO nanoparticles induce apoptosis in cancer cells and exhibit potential as a promising anticancer agent.</p><h2>Other Information</h2> <p> Published in: Heliyon<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.heliyon.2023.e15560" target="_blank">https://dx.doi.org/10.1016/j.heliyon.2023.e15560</a></p>
eu_rights_str_mv openAccess
id Manara2_cf65bf456e3c16fc986f8144f2a2bfde
identifier_str_mv 10.1016/j.heliyon.2023.e15560
network_acronym_str Manara2
network_name_str Manara2
oai_identifier_str oai:figshare.com:article/25059731
publishDate 2023
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spelling Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticlesMohamed Qasim Al-Fahdawi (17844209)Ahmed Faris Aldoghachi (16301714)Fatah H. Alhassan (17844212)Faris A.J. Al-Doghachi (17844215)Hussah Abdullah Alshwyeh (16621140)Abdullah Rasedee (6940799)Sulaiman Mohammed Alnasser (16713520)Mothanna Sadiq Al-Qubaisi (17844218)Wisam Nabeel Ibrahim (13899337)Biomedical and clinical sciencesClinical sciencesPharmacology and pharmaceutical sciencesAg/MgO nanoparticlesHT29 cellA549 cellAntiproliferativeApoptosis<p>Silver-doped magnesia nanoparticles (Ag/MgO) were synthesized using the precipitation method and characterized by various techniques such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermal gravimetric analysis (TGA), Brunner-Emmett-Teller (BET) surface area measurements, and dispersive X-ray spectroscopy (EDX). The morphology of Ag/MgO nanoparticles was determined by transmission and scanning electron microscopy, which revealed cuboidal shaped nanoparticles with sizes ranging from 31 to 68 nm and an average size of 43.5 ± 10.6 nm. The anticancer effects of Ag/MgO nanoparticles were evaluated on human colorectal (HT29) and lung adenocarcinoma (A549) cell lines, and their caspase-3, -8, and -9 activities, as well as Bcl-2, Bax, p53, cytochrome C protein expressions were estimated. Ag/MgO nanoparticles showed selective toxicity towards HT29 and A549 cells while remaining relatively innocuous towards the normal human colorectal, CCD-18Co, and lung, MRC-5 cells. The IC50 values of Ag/MgO nanoparticles on the HT29 and A549 cells were found to be 90.2 ± 2.6 and 85.0 ± 3.5 μg/mL, respectively. The Ag/MgO nanoparticles upregulated caspase-3 and -9 activities, downregulated Bcl-2, upregulated Bax and p53 protein expressions in the cancer cells. The morphology of the Ag/MgO nanoparticle treated HT29 and A549 cells was typical of apoptosis, with cell detachment, shrinkage, and membrane blebbing. The results suggest that Ag/MgO nanoparticles induce apoptosis in cancer cells and exhibit potential as a promising anticancer agent.</p><h2>Other Information</h2> <p> Published in: Heliyon<br> License: <a href="http://creativecommons.org/licenses/by/4.0/" target="_blank">http://creativecommons.org/licenses/by/4.0/</a><br>See article on publisher's website: <a href="https://dx.doi.org/10.1016/j.heliyon.2023.e15560" target="_blank">https://dx.doi.org/10.1016/j.heliyon.2023.e15560</a></p>2023-04-17T03:00:00ZTextJournal contributioninfo:eu-repo/semantics/publishedVersiontextcontribution to journal10.1016/j.heliyon.2023.e15560https://figshare.com/articles/journal_contribution/Physicochemical_characterization_and_cancer_cell_antiproliferative_effect_of_silver-doped_magnesia_nanoparticles/25059731CC BY 4.0info:eu-repo/semantics/openAccessoai:figshare.com:article/250597312023-04-17T03:00:00Z
spellingShingle Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles
Mohamed Qasim Al-Fahdawi (17844209)
Biomedical and clinical sciences
Clinical sciences
Pharmacology and pharmaceutical sciences
Ag/MgO nanoparticles
HT29 cell
A549 cell
Antiproliferative
Apoptosis
status_str publishedVersion
title Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles
title_full Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles
title_fullStr Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles
title_full_unstemmed Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles
title_short Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles
title_sort Physicochemical characterization and cancer cell antiproliferative effect of silver-doped magnesia nanoparticles
topic Biomedical and clinical sciences
Clinical sciences
Pharmacology and pharmaceutical sciences
Ag/MgO nanoparticles
HT29 cell
A549 cell
Antiproliferative
Apoptosis