Operando Analysis of Nickel Catalyst Speciation in Reductive Biaryl Synthesis Using Thin Layer Electrochemistry and a Microelectrode

Operando Analysis of Nickel Catalyst Speciation in Reductive Biaryl Synthesis Using Thin Layer Electrochemistry and a Microelectrode

Operando insights into nickel speciation during nickel-catalyzed cross-electrophile coupling reactions could play a major role in advancing these reactions, but analytical methods capable of providing such insights have not yet been developed. In this study, we integrate a thin-layer electrode (TLE)...

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Autore principale: Buwanila T. Punchihewa (22688305) (author)
Altri autori: Antonio Romero-Arenas (3110208) (author), Robert S. Paton (1281666) (author), Daniel J. Weix (1284837) (author), Shannon S. Stahl (1291731) (author), Mohammad Rafiee (1474582) (author)
Pubblicazione: 2025
Soggetti:
Biochemistry
Medicine
Ecology
Infectious Diseases
Environmental Sciences not elsewhere classified
Biological Sciences not elsewhere classified
analytical methods capable
enable operando monitoring
ii </ sup
nickel catalyst speciation
microelectrode operando insights
catalyst speciation
operando analysis
nickel speciation
yielding insight
temporal evolution
results establish
reductive homocoupling
major role
layer electrode
kinetic profiles
including accumulation
different quantities
catalyzed cross
bipyridyl ligand
based intermediates
aryl halides
approach allows
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