Operando Heating and Cooling Electrochemical 4D-STEM Probing Nanoscale Dynamics at Solid–Liquid Interfaces

Operando/in situ methods have revolutionized our fundamental understanding of molecular and structural changes at solid–liquid interfaces and enabled the vision of “watching chemistry in action”. Operando transmission electron microscopy (TEM)...

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Main Author:	Sungin Kim (7534526) (author)
Other Authors:	Valentin Briega-Martos (20749946) (author), Shikai Liu (245897) (author), Kwanghwi Je (14289535) (author), Chuqiao Shi (8721630) (author), Katherine Marusak Stephens (21414527) (author), Steven E. Zeltmann (8350224) (author), Zhijing Zhang (297460) (author), Rafael Guzman-Soriano (21414530) (author), Wenqi Li (137889) (author), Jiahong Jiang (781283) (author), Juhyung Choi (11809596) (author), Yafet J. Negash (21414533) (author), Franklin S. Walden (21414536) (author), Nelson L. Marthe (21414539) (author), Patrick S. Wellborn (21414542) (author), Yaofeng Guo (21414545) (author), John Damiano (1420231) (author), Yimo Han (1661224) (author), Erik H. Thiede (9029096) (author), Yao Yang (543059) (author)
Published:	2025
Subjects:	Biotechnology Space Science Biological Sciences not elsewhere classified Chemical Sciences not elsewhere classified Physical Sciences not elsewhere classified “ watching chemistry work benchmarked electrochemistry used cu electrodeposition transmission electron microscopy scale cu dendrites resolved nanoscale dynamics g ., catalysts despite early reports demonstrate quantitative electrochemistry controlled nanoscale electrochemistry assisted quantitative 4d 95 ° c 300 ° c 1 v vs standard hydrogen electrode electrode thermal circuit thermal control remains random orientations followed pt pseudoreference electrode wide temperature range electrode electrochemical circuit cooling electrochemical 4d 8 ± 0 cooling electrochemical liquid stem structural analysis cell scanning tem understanding fundamental temperature fundamental understanding structural changes remains ph pt pseudo preferential orientations cell tem electrode ec simultaneous electrochemical cooling ec room temperature − 50 − 40 systematically investigated stripping processes steady states stage growth situ </ reliable potential realistic climates powerful tool ph dependence organic solutions operando </
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<i>Operando</i> Heating and Cooling Electrochemical 4D-STEM Probing Nanoscale Dynamics at Solid–Liquid Interfaces

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