Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water

Produced water contaminated with oil has adverse effects on human health and aquatic life. Providing an efficient method for the removal of oil from produced water is a challenging task. In this study, the effects of carbon chain length and the cation nature of ionic liquids (ILs) on the removal eff...

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محفوظ في:
التفاصيل البيبلوغرافية
المؤلف الرئيسي: Liaqat, Shehzad (author)
مؤلفون آخرون: Khan, Amir (author), Akbar, Noor (author), Ibrahim, Mustafa (author), Khamis, Mustafa (author), Nancarrow, Paul (author), Siddiqui, Ruqaiyyah (author), Khan, Naveed (author), Abouleish, Mohamed (author)
التنسيق: article
منشور في: 2022
الموضوعات:
الوصول للمادة أونلاين:https://hdl.handle.net/11073/33271
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author Liaqat, Shehzad
author2 Khan, Amir
Akbar, Noor
Ibrahim, Mustafa
Khamis, Mustafa
Nancarrow, Paul
Siddiqui, Ruqaiyyah
Khan, Naveed
Abouleish, Mohamed
author2_role author
author
author
author
author
author
author
author
author_facet Liaqat, Shehzad
Khan, Amir
Akbar, Noor
Ibrahim, Mustafa
Khamis, Mustafa
Nancarrow, Paul
Siddiqui, Ruqaiyyah
Khan, Naveed
Abouleish, Mohamed
author_role author
dc.creator.none.fl_str_mv Liaqat, Shehzad
Khan, Amir
Akbar, Noor
Ibrahim, Mustafa
Khamis, Mustafa
Nancarrow, Paul
Siddiqui, Ruqaiyyah
Khan, Naveed
Abouleish, Mohamed
dc.date.none.fl_str_mv 2022
2026-04-01T09:37:56Z
2026-04-01T09:37:56Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv Liaqat, S., Khan, A. S., Akbar, N., Ibrahim, T. H., Khamis, M. I., Nancarrow, P., Siddiqui, R., Khan, N. A., & Abouleish, M. Y. (2022). Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water. Processes, 10(9), 1897. https://doi.org/10.3390/pr10091897
2227-9717
https://hdl.handle.net/11073/33271
10.3390/pr10091897
dc.language.none.fl_str_mv en
dc.publisher.none.fl_str_mv MDPI
dc.relation.none.fl_str_mv https://doi.org/10.3390/pr10091897
dc.rights.none.fl_str_mv Attribution 4.0 International
http://creativecommons.org/licenses/by/4.0/
dc.subject.none.fl_str_mv Produced Water
Oil Removal
Ionic Liquids
Liquid–Liquid Extraction
dc.title.none.fl_str_mv Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water
dc.type.none.fl_str_mv Peer-Reviewed
Published version
info:eu-repo/semantics/publishedVersion
info:eu-repo/semantics/article
description Produced water contaminated with oil has adverse effects on human health and aquatic life. Providing an efficient method for the removal of oil from produced water is a challenging task. In this study, the effects of carbon chain length and the cation nature of ionic liquids (ILs) on the removal efficiency of oil from produced water were investigated. For this purpose, seven ILs containing the bis (trifluoromethylsulfonyl) imide (NTf2) anion, and various cations such as imidazolium, pyridinium, phosphonium, and ammonium, were employed for the removal of oil from produced water via liquid–liquid extraction. The effects of process parameters such as the initial concentration of oil in produced water, contact time, pH, salinity, phase ratio, and temperature on the removal efficiency of oil were studied and optimized. 1-Decyl-3-methyl-imidazolium bis(trifluoromethylsulfonyl)imide ([C10mim][NTf2]) (IL4) was found to give the highest oil extraction efficiency of 92.8% under optimum conditions. The extraction efficiency was found to increase with increasing cation alkyl chain length from C2 to C10. The extraction efficiency of ILs based on cations follows the order imidazolium > ammonium > phosphonium > anpyridinium. Fourier Transform infrared spectroscopy (FTIR) was used to explore the ILs interaction with oil using [C10mim][NTf2] as a model. In addition, 1H and 13C NMR spectra were recorded to obtain a better understanding of the molecular structure of IL and to investigate the peak shifts in H and C atoms. Moreover, the cell viability of the most efficient IL, [C10mim][NTf2], in human cells was investigated. It has been concluded that this IL exhibited minimal cytotoxic effects at lower concentrations against human cell lines and is effective for the extraction of oil from aqueous media.
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identifier_str_mv Liaqat, S., Khan, A. S., Akbar, N., Ibrahim, T. H., Khamis, M. I., Nancarrow, P., Siddiqui, R., Khan, N. A., & Abouleish, M. Y. (2022). Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water. Processes, 10(9), 1897. https://doi.org/10.3390/pr10091897
2227-9717
10.3390/pr10091897
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spelling Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced WaterLiaqat, ShehzadKhan, AmirAkbar, NoorIbrahim, MustafaKhamis, MustafaNancarrow, PaulSiddiqui, RuqaiyyahKhan, NaveedAbouleish, MohamedProduced WaterOil RemovalIonic LiquidsLiquid–Liquid ExtractionProduced water contaminated with oil has adverse effects on human health and aquatic life. Providing an efficient method for the removal of oil from produced water is a challenging task. In this study, the effects of carbon chain length and the cation nature of ionic liquids (ILs) on the removal efficiency of oil from produced water were investigated. For this purpose, seven ILs containing the bis (trifluoromethylsulfonyl) imide (NTf2) anion, and various cations such as imidazolium, pyridinium, phosphonium, and ammonium, were employed for the removal of oil from produced water via liquid–liquid extraction. The effects of process parameters such as the initial concentration of oil in produced water, contact time, pH, salinity, phase ratio, and temperature on the removal efficiency of oil were studied and optimized. 1-Decyl-3-methyl-imidazolium bis(trifluoromethylsulfonyl)imide ([C10mim][NTf2]) (IL4) was found to give the highest oil extraction efficiency of 92.8% under optimum conditions. The extraction efficiency was found to increase with increasing cation alkyl chain length from C2 to C10. The extraction efficiency of ILs based on cations follows the order imidazolium > ammonium > phosphonium > anpyridinium. Fourier Transform infrared spectroscopy (FTIR) was used to explore the ILs interaction with oil using [C10mim][NTf2] as a model. In addition, 1H and 13C NMR spectra were recorded to obtain a better understanding of the molecular structure of IL and to investigate the peak shifts in H and C atoms. Moreover, the cell viability of the most efficient IL, [C10mim][NTf2], in human cells was investigated. It has been concluded that this IL exhibited minimal cytotoxic effects at lower concentrations against human cell lines and is effective for the extraction of oil from aqueous media.MDPI2026-04-01T09:37:56Z2026-04-01T09:37:56Z2022Peer-ReviewedPublished versioninfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfLiaqat, S., Khan, A. S., Akbar, N., Ibrahim, T. H., Khamis, M. I., Nancarrow, P., Siddiqui, R., Khan, N. A., & Abouleish, M. Y. (2022). Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water. Processes, 10(9), 1897. https://doi.org/10.3390/pr100918972227-9717https://hdl.handle.net/11073/3327110.3390/pr10091897enhttps://doi.org/10.3390/pr10091897Attribution 4.0 Internationalhttp://creativecommons.org/licenses/by/4.0/oai:repository.aus.edu:11073/332712026-04-02T05:14:52Z
spellingShingle Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water
Liaqat, Shehzad
Produced Water
Oil Removal
Ionic Liquids
Liquid–Liquid Extraction
status_str publishedVersion
title Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water
title_full Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water
title_fullStr Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water
title_full_unstemmed Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water
title_short Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water
title_sort Hydrophobic Ionic Liquids for Efficient Extraction of Oil from Produced Water
topic Produced Water
Oil Removal
Ionic Liquids
Liquid–Liquid Extraction
url https://hdl.handle.net/11073/33271